Quality testing competence in sauce and fish sauce (04/03/2015)

No

CRITERIA

TEST METHOD

LOD

I. ORGANOLEPTIC

1.        

Apperance

Organoleptic

-

2.        

Odor

Organoleptic

-

3.        

Flavor

Organoleptic

-           

4.        

Color

Organoleptic

-           

5.        

Visible impurrties (**)

Organoleptic

-           

II. QUALITY INGREDIENT

6.        

Độ acid (theo acid acetic)(**)

TCVN 3702:2009

0.01 g/100mL

7.        

Carbohydrate

Calculate (Included testing Moisture, Ash, Fat, Protein),
Food Composition

%wt

8.        

Muối (NaCl)

AOAC 937.09

0.005 g/100mL

9.        

Protein

TCVN 3705:1990 (*) AOAC 940.25:2005 (*)

% wt

10.     

Nito ammoniac

TCVN 3706:1990

mg/100g

11.     

Nito acid amin(**)

TCVN 3708:1990

0.05 g/100mL

12.     

Nito formol(**)

TCVN 3707:1990

0.05 g/100mL

13.     

Hàm lượng chất khô

FAO, 14/7, 1986

0.02 g/100mL

14.     

Béo

FAO 14/7 p. 212, 1986

%wt

15.     

Nito amin(**)

TCVN 3707:1990

0.05 g/100mL

16.     

Urê(**)

TK. Appilication Note SSI – AP – LCMS 0277 – Shimadzu (LCMSMS)

0.2mg/l

17.     

Histamine(**)

TK. EZ : faast (LCMSMS)

1.0 mg/l

18.     

Acid amine (gồm 20 acid amine)(**)

TK.EZ : faast (LCMSMS)

10.0 mg/kg

19.     

Glycine(**)

TK.EZ : faast (LCMSMS)

10.0 mg/kg

 

Alanine(**)

 

10.0 mg/l

 

Serine(**)

 

10.0 mg/l

 

Proline(**)

 

10.0 mg/l

 

Valine(**)

 

10.0 mg/l

 

Threonine(**)

 

10.0 mg/l

 

Methionine(**)

 

10.0 mg/l

 

Trans-4-hydroxy-proline(**)

 

10.0 mg/l

 

Arginine(**)

 

10.0 mg/l

 

Aspartic acid(**)

 

10.0 mg/l

 

Glutamic acid(**)

 

10.0 mg/l

 

Cysteine(**)

 

10.0 mg/l

 

Lysine(**)

 

10.0 mg/l

 

Histidine(**)

 

10.0 mg/l

 

Tyrosine(**)

 

10.0 mg/l

 

Cystine(**)

 

10.0 mg/l

 

Leucine _ Isoleucine(**)

 

10.0 mg/l

 

Phenylalamine(**)

 

10.0 mg/l

III. QUANTITIES OF VITAMIN

20.     

Vitamine A(**)

TK.AOAC 992.06:2011 (HPLC.UV)

0.1mg/l

21.     

Vitamine D3(**)

TK.AOAC 992.06:2011 (HPLC.UV)

0.1mg/l

22.     

Vitamin E(**)

TK.AOAC 992.06:2011 (HPLC.UV)

0.1mg/l

23.     

Vitamin C

Ref Journal of Chromatography A
UHPLC-DAD

ppb

24.     

Vitamin B1

TK.AOAC 985.33:2011 (HPLC-UV)

0.1mg/l

25.     

Vitamin B2

Ref Journal of Chromatography A

0.1mg/l

26.     

Vitamin B3 (Nicotinamide)

TK.AOAC 985.33:2011 (HPLC-UV)

0.1mg/l

27.     

Vitamin B5 (Acid pantothenic)

TK.AOAC 985.33:2011 (HPLC-UV)

0.1mg/l

28.     

Vitamin B6

TK.AOAC 985.33:2011 (HPLC-UV)

0.1mg/l

29.     

Vitamin B9 (Floic acid)

TK.AOAC 985.33:2011 (HPLC-UV)

0.1mg/l

30.     

Vitamine B12

TK.AOAC 985.33:2011 (HPLC-UV)

0.1mg/l

31.     

Biotin(**)

TK.AOAC 985.33:2011 (HPLC-UV)

0.1mg/l

IV. PRESERVATION

32.     

Sunfua dioxite (SO2)

AOAC 962.16

2(mg/kg)

33.     

Acid citric (E330)

Ref Megazyme International Ireland 2012
UHPLC-DAD

ppb

34.     

Acid Tartaric (E334)(**)

TK. US EPA method 300.00(IC)

20.0mg/l

35.     

Acid malic (E296)(**)

TK. US EPA method 300.00(IC)

20.0mg/l

36.     

Acid fumaric (E297)(**)

TK. US EPA method 300.00(IC)

20.0mg/l

37.     

Acid lactic (E270)(**)

TK. US EPA method 300.00(IC)

20.0mg/l

38.     

Acid ascorbic / Natri ascorbate

Ref Journal of Chromatography A
UHPLC-DAD

ppb

39.     

Alpha-Tocopherol(**)

TK : AOAC 992.06 (HPLC/UV)

0.1mg/l

40.     

BHA (Butylated hydroxyanisol)(**)

TK : AOAC 983.15 (HPLC/UV)

5.0mg/l

41.     

BHT (Butylated hydroxytoluene)(**)

TK : AOAC 983.15 (HPLC/UV)

5.0mg/l

42.     

TBHQ (Tert-Butyl hydroquinone)(**)

TK : AOAC 983.15 (HPLC/UV)

5.0mg/l

43.     

Natri benzoate / Acid benzoic

Ref Journal of chromatography A, 1073(2005) 393 – 397
UHPLC-DAD

ppb

44.     

Kali sorabte/ Acid sorbic

Ref Journal of Chromatography A
UHPLC-DAD

ppb

V. QUANTITIES OF ADDITIVES AND ADDED CHEMICAL

45.     

Aspartame (E951)(**)

TK. TCVN 8471 : 2010 (HPLC/UV)

10mg/l

46.     

Acesulfam K (E950)(**)

TK. TCVN 8471 : 2010 (HPLC/UV)

10mg/l

47.     

Saccharine (E954)(**)

TK. TCVN 8471 : 2010 (HPLC/UV)

0.5mg/l

48.     

Cyclamate (E952)(**)

TK. US EPA method 300.00(IC)

20.0mg/l

49.     

Monosodium Glutamate(**)

TK. EZ : faast (LCMSMS)

10.0mg/l

50.     

Disodium Isosinate(**)

TK : HPLC Application Note 820435 (HPLC/UV)

5.0mg/l

51.     

Disodium Guanylate(**)

TK : HPLC Application Note 820435 (HPLC/UV)

5.0mg/l

52.     

Beta-caroten(**)

TK : AOAC 992.06 (HPLC/UV)

0.1mg/l

53.     

Curcumin(**)

(HPLC/UV)

10.0mg/l

54.     

Lycopen(**)

TK.AOAC 992.06:2011 (HPLC.UV)

0.1mg/l

55.     

Orange II(**)

TK : LGC/GC/2007/005 Analysis of illegal Dyes in chilli Powder by LC-UV (HPLC/UV

0.1mg/l

56.     

Parared(**)

TK : LGC/GC/2007/005 Analysis of illegal Dyes in chilli Powder by LC-UV (HPLC/UV

0.1mg/l

57.     

Ponceau 4R(**)

TK : LGC/GC/2007/005 Analysis of illegal Dyes in chilli Powder by LC-UV (HPLC/UV

10.mg/l

58.     

Rhodamine B(**)

TK : Method No PV 2072, OSHA, USD (HPLC/UV)

0.1mg/l

59.     

Riboflavin(**)

TK : AOAC 992.06 (HPLC/UV)

0.1mg/l

60.     

Sudan(**)

TK : AOAC International Workshop " Food to Dyes For" (HPLC/UV)

0.1mg/l

61.     

Sudan I(**)

0.1mg/l

62.     

Sudan II(**)

0.1mg/l

63.     

Sudan III(**)

0.1mg/l

64.     

Sudan IV(**)

0.1mg/l

65.     

Sunset yellow(**)

TK : JFDA Vol 14, No3, 2006, P284 – 291 (HPLC/UV)

10.0mg/l

66.     

Tartazine(**)

TK : JFDA Vol 14, No3, 2006, P284 – 291 (HPLC/UV)

10.0mg/l

VI. NITRIT AND NITRAT RESIDUES

67.     

Nitrit (NO2-)(**)

TK.TCVN 7767:2007

1 mg/L

68.     

Nitrat (NO3-)(**)

TK.TCVN 7767:2007

1 mg/L

VII. HEAVY METAL AND OTHER METAL

69.     

As

Ref. AOAC986.15

 mg/L

70.     

Hg(**)

Ref. AOAC986.15

 mg/L

71.     

Cd

AOAC 999.11

 mg/L

72.     

Pb

AOAC 999.11

 mg/L

73.     

Cu

AOAC 999.11

 mg/L

74.     

Ca

AOAC 969.23

 mg/L

75.     

Se

Ref. AOAC986.15

 mg/L

76.     

Fe

AOAC 999.11

 mg/L

77.     

Na

AOAC 969.23

 mg/L

78.     

Zn

AOAC 999.11

 mg/L

79.     

Sb

Ref. AOAC986.15

 mg/L

80.     

Borat

Ref. 3390/2000/QĐ-BYT

 mg/L

81.     

P2O5

Ref. EPA method 200.7

 mg/L

VIII. PLANT PROTECTION DRUG RESIDUES

83.     

Clo plant protection drug residues

TK.AOAC 2007.01 (LCMSMS)

-

 

2,4'-DDD

0.05mg/l

 

4,4'-DDE

0.05mg/l

 

2,4'-DDE

0.05mg/l

 

Alpha-Lindan

0.05mg/l

 

Gamma-Lindan

0.05mg/l

 

Beta-Lindan

0.05mg/l

 

Isodrin

0.05mg/l

 

Aldrin

0.05mg/l

 

Dieldrin

0.05mg/l

 

Hexachloro-Benzene

0.05mg/l

 

Heptachlor

0.05mg/l

 

Heptachlor epoxide

0.05mg/l

 

Endosulfan I

0.05mg/l

85.     

Phosphor Pesticide

TK.AOAC 2007.01 (LCMSMS)

-

 

Fenthion

0.05mg/l

 

Diazinon

0.05mg/l

 

Parathion Methyl

0.05mg/l

 

Malathion

0.05mg/l

 

Chlorpyrifos

0.05mg/l

 

Parathion ethyl

0.05mg/l

 

Bromophos methyl

0.05mg/l

 

Bromophos ethyl

0.05mg/l

 

Ethion

0.05mg/l

86.     

Chrysanthemum Pesticide

TK.AOAC 2007.01 (LCMSMS)

0.05mg/l

 

Cypermethrin

0.05mg/l

 

Deltamethrin

0.05mg/l

 

Permethrin

0.05mg/l

 

Fenvalerate

0.05mg/l

 

Resmethrine

0.05mg/l

 

Fenthropathrine

0.05mg/l

87.     

Carbamate Pesticide

TK.AOAC 2007.01 (LCMSMS)

 

 

Isoprocarb

0.01mg/l

 

Aldicarb sulfone

0.01mg/l

 

Aldicarb

0.01mg/l

 

Aldicarb sulfoxide

0.01mg/l

 

Propoxur

0.01mg/l

 

Carbofuran

0.01mg/l

 

Carbaryl

0.01mg/l

 

Methomyl

0.01mg/l

 

Oxamyl

0.01mg/l

 

Thiodicarb

0.01mg/l

 

Methiocarb

0.01mg/l

 

Fenobucarb

0.01mg/l

 

Propoxur

0.01mg/l

 

Carbofuran-3-Hydroxy

0.01mg/l

IX. MYCOTOXIN

88.     

Aflatoxin Tổng(**)

TK.AOAC 991.31 (LC/MS/MS)

1.0µg/l

89.     

Aflatoxin/chất (B1, B2, G1, G2)(**)

TK.AOAC 991.31(LC/MS/MS)

1.0µg/l

90.     

Ochratoxin A(**)

TK. AOAC 2000.09(LC/MS/MS)

1.0µg/l

91.     

Deoxynivalenol (DON)(**)

TK.AOAC 986.18 (LC/MS/MS)

100µg/l

92.     

Zearalenone(**)

TK .Analytical Chimica Acta 487, p137-143 (LC/MS/MS)

1.0µg/l

X. MICROBIOLOGY

A.     

TPC

ISO 4833-1:2013

CFU/G

93

Enterobacteriaceae

ISO 21528-2:2004

CFU/G

94

Coliform

ISO 4832:2006

CFU/G

95

E. coli

ISO 16649-2:2001

CFU/G

96

E. coli

ISO 7251:2005

MPN/G; /G

97

Staphylococcus positive coagulase

ISO 6888-1:1999

CFU/G

98

Staphylococcus aureus

ISO 6888-1:1999

CFU/G

99

Salmonella

ISO 6579:2002

/25G

100

Vibrio parahaemolyticus

ISO 21872-1:2007

/25G

101

Vibrio cholerae

ISO 21872-1:2007

/25G

102

Listeria monocytogenes

ISO 11290-1:1996/ Amd.1:2004

/25G

103

Total yeast - mould

ISO 21527-1&2: 2008

CFU/G

104

Clostridium perfringens

ISO 7937:2004

CFU/G

105

Spores of sulfite-reducing anaerobes (Clostridia)

ISO 15213:2003

CFU/G

Note:

TCVN : Vietnam Standards                           

AOAC: Association of Official Analytical Chemist (USA)                            

FAO: Food and Agriculture Organization                        

(**) Criteria  is performed by subcontractor

TK: Normative references

Criteria are not included in this table will agree the development and application with customers about method

Released time:

5 working days. In special case, depending on the requirements of customers will be agreed later.

Vinacert willing to perform the services and return the results on holidays as agreement with customer.

Representative sample volume: 800 grams    

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