|
No
|
CRITERIA
|
TEST METHOD
|
LOD
|
|
I. ORGANOLEPTIC
|
|
1.
|
Apperance
|
Organoleptic
|
-
|
|
2.
|
Odor
|
Organoleptic
|
-
|
|
3.
|
Flavor
|
Organoleptic
|
-
|
|
4.
|
Color
|
Organoleptic
|
-
|
|
5.
|
Visible impurrties (**)
|
Organoleptic
|
-
|
|
II. QUALITY INGREDIENT
|
|
6.
|
Độ acid (theo acid acetic)(**)
|
TCVN 3702:2009
|
0.01 g/100mL
|
|
7.
|
Carbohydrate
|
Calculate (Included testing Moisture, Ash, Fat, Protein),
Food Composition
|
%wt
|
|
8.
|
Muối (NaCl)
|
AOAC 937.09
|
0.005 g/100mL
|
|
9.
|
Protein
|
TCVN 3705:1990 (*) AOAC 940.25:2005 (*)
|
% wt
|
|
10.
|
Nito ammoniac
|
TCVN 3706:1990
|
mg/100g
|
|
11.
|
Nito acid amin(**)
|
TCVN 3708:1990
|
0.05 g/100mL
|
|
12.
|
Nito formol(**)
|
TCVN 3707:1990
|
0.05 g/100mL
|
|
13.
|
Hàm lượng chất khô
|
FAO, 14/7, 1986
|
0.02 g/100mL
|
|
14.
|
Béo
|
FAO 14/7 p. 212, 1986
|
%wt
|
|
15.
|
Nito amin(**)
|
TCVN 3707:1990
|
0.05 g/100mL
|
|
16.
|
Urê(**)
|
TK. Appilication Note SSI – AP – LCMS 0277 – Shimadzu (LCMSMS)
|
0.2mg/l
|
|
17.
|
Histamine(**)
|
TK. EZ : faast (LCMSMS)
|
1.0 mg/l
|
|
18.
|
Acid amine (gồm 20 acid amine)(**)
|
TK.EZ : faast (LCMSMS)
|
10.0 mg/kg
|
|
19.
|
Glycine(**)
|
TK.EZ : faast (LCMSMS)
|
10.0 mg/kg
|
|
|
Alanine(**)
|
|
10.0 mg/l
|
|
|
Serine(**)
|
|
10.0 mg/l
|
|
|
Proline(**)
|
|
10.0 mg/l
|
|
|
Valine(**)
|
|
10.0 mg/l
|
|
|
Threonine(**)
|
|
10.0 mg/l
|
|
|
Methionine(**)
|
|
10.0 mg/l
|
|
|
Trans-4-hydroxy-proline(**)
|
|
10.0 mg/l
|
|
|
Arginine(**)
|
|
10.0 mg/l
|
|
|
Aspartic acid(**)
|
|
10.0 mg/l
|
|
|
Glutamic acid(**)
|
|
10.0 mg/l
|
|
|
Cysteine(**)
|
|
10.0 mg/l
|
|
|
Lysine(**)
|
|
10.0 mg/l
|
|
|
Histidine(**)
|
|
10.0 mg/l
|
|
|
Tyrosine(**)
|
|
10.0 mg/l
|
|
|
Cystine(**)
|
|
10.0 mg/l
|
|
|
Leucine _ Isoleucine(**)
|
|
10.0 mg/l
|
|
|
Phenylalamine(**)
|
|
10.0 mg/l
|
|
III. QUANTITIES OF VITAMIN
|
|
20.
|
Vitamine A(**)
|
TK.AOAC 992.06:2011 (HPLC.UV)
|
0.1mg/l
|
|
21.
|
Vitamine D3(**)
|
TK.AOAC 992.06:2011 (HPLC.UV)
|
0.1mg/l
|
|
22.
|
Vitamin E(**)
|
TK.AOAC 992.06:2011 (HPLC.UV)
|
0.1mg/l
|
|
23.
|
Vitamin C
|
Ref Journal of Chromatography A
UHPLC-DAD
|
ppb
|
|
24.
|
Vitamin B1
|
TK.AOAC 985.33:2011 (HPLC-UV)
|
0.1mg/l
|
|
25.
|
Vitamin B2
|
Ref Journal of Chromatography A
|
0.1mg/l
|
|
26.
|
Vitamin B3 (Nicotinamide)
|
TK.AOAC 985.33:2011 (HPLC-UV)
|
0.1mg/l
|
|
27.
|
Vitamin B5 (Acid pantothenic)
|
TK.AOAC 985.33:2011 (HPLC-UV)
|
0.1mg/l
|
|
28.
|
Vitamin B6
|
TK.AOAC 985.33:2011 (HPLC-UV)
|
0.1mg/l
|
|
29.
|
Vitamin B9 (Floic acid)
|
TK.AOAC 985.33:2011 (HPLC-UV)
|
0.1mg/l
|
|
30.
|
Vitamine B12
|
TK.AOAC 985.33:2011 (HPLC-UV)
|
0.1mg/l
|
|
31.
|
Biotin(**)
|
TK.AOAC 985.33:2011 (HPLC-UV)
|
0.1mg/l
|
|
IV. PRESERVATION
|
|
32.
|
Sunfua dioxite (SO2)
|
AOAC 962.16
|
2(mg/kg)
|
|
33.
|
Acid citric (E330)
|
Ref Megazyme International Ireland 2012
UHPLC-DAD
|
ppb
|
|
34.
|
Acid Tartaric (E334)(**)
|
TK. US EPA method 300.00(IC)
|
20.0mg/l
|
|
35.
|
Acid malic (E296)(**)
|
TK. US EPA method 300.00(IC)
|
20.0mg/l
|
|
36.
|
Acid fumaric (E297)(**)
|
TK. US EPA method 300.00(IC)
|
20.0mg/l
|
|
37.
|
Acid lactic (E270)(**)
|
TK. US EPA method 300.00(IC)
|
20.0mg/l
|
|
38.
|
Acid ascorbic / Natri ascorbate
|
Ref Journal of Chromatography A
UHPLC-DAD
|
ppb
|
|
39.
|
Alpha-Tocopherol(**)
|
TK : AOAC 992.06 (HPLC/UV)
|
0.1mg/l
|
|
40.
|
BHA (Butylated hydroxyanisol)(**)
|
TK : AOAC 983.15 (HPLC/UV)
|
5.0mg/l
|
|
41.
|
BHT (Butylated hydroxytoluene)(**)
|
TK : AOAC 983.15 (HPLC/UV)
|
5.0mg/l
|
|
42.
|
TBHQ (Tert-Butyl hydroquinone)(**)
|
TK : AOAC 983.15 (HPLC/UV)
|
5.0mg/l
|
|
43.
|
Natri benzoate / Acid benzoic
|
Ref Journal of chromatography A, 1073(2005) 393 – 397
UHPLC-DAD
|
ppb
|
|
44.
|
Kali sorabte/ Acid sorbic
|
Ref Journal of Chromatography A
UHPLC-DAD
|
ppb
|
|
V. QUANTITIES OF ADDITIVES AND ADDED CHEMICAL
|
|
45.
|
Aspartame (E951)(**)
|
TK. TCVN 8471 : 2010 (HPLC/UV)
|
10mg/l
|
|
46.
|
Acesulfam K (E950)(**)
|
TK. TCVN 8471 : 2010 (HPLC/UV)
|
10mg/l
|
|
47.
|
Saccharine (E954)(**)
|
TK. TCVN 8471 : 2010 (HPLC/UV)
|
0.5mg/l
|
|
48.
|
Cyclamate (E952)(**)
|
TK. US EPA method 300.00(IC)
|
20.0mg/l
|
|
49.
|
Monosodium Glutamate(**)
|
TK. EZ : faast (LCMSMS)
|
10.0mg/l
|
|
50.
|
Disodium Isosinate(**)
|
TK : HPLC Application Note 820435 (HPLC/UV)
|
5.0mg/l
|
|
51.
|
Disodium Guanylate(**)
|
TK : HPLC Application Note 820435 (HPLC/UV)
|
5.0mg/l
|
|
52.
|
Beta-caroten(**)
|
TK : AOAC 992.06 (HPLC/UV)
|
0.1mg/l
|
|
53.
|
Curcumin(**)
|
(HPLC/UV)
|
10.0mg/l
|
|
54.
|
Lycopen(**)
|
TK.AOAC 992.06:2011 (HPLC.UV)
|
0.1mg/l
|
|
55.
|
Orange II(**)
|
TK : LGC/GC/2007/005 Analysis of illegal Dyes in chilli Powder by LC-UV (HPLC/UV
|
0.1mg/l
|
|
56.
|
Parared(**)
|
TK : LGC/GC/2007/005 Analysis of illegal Dyes in chilli Powder by LC-UV (HPLC/UV
|
0.1mg/l
|
|
57.
|
Ponceau 4R(**)
|
TK : LGC/GC/2007/005 Analysis of illegal Dyes in chilli Powder by LC-UV (HPLC/UV
|
10.mg/l
|
|
58.
|
Rhodamine B(**)
|
TK : Method No PV 2072, OSHA, USD (HPLC/UV)
|
0.1mg/l
|
|
59.
|
Riboflavin(**)
|
TK : AOAC 992.06 (HPLC/UV)
|
0.1mg/l
|
|
60.
|
Sudan(**)
|
TK : AOAC International Workshop " Food to Dyes For" (HPLC/UV)
|
0.1mg/l
|
|
61.
|
Sudan I(**)
|
0.1mg/l
|
|
62.
|
Sudan II(**)
|
0.1mg/l
|
|
63.
|
Sudan III(**)
|
0.1mg/l
|
|
64.
|
Sudan IV(**)
|
0.1mg/l
|
|
65.
|
Sunset yellow(**)
|
TK : JFDA Vol 14, No3, 2006, P284 – 291 (HPLC/UV)
|
10.0mg/l
|
|
66.
|
Tartazine(**)
|
TK : JFDA Vol 14, No3, 2006, P284 – 291 (HPLC/UV)
|
10.0mg/l
|
|
VI. NITRIT AND NITRAT RESIDUES
|
|
67.
|
Nitrit (NO2-)(**)
|
TK.TCVN 7767:2007
|
1 mg/L
|
|
68.
|
Nitrat (NO3-)(**)
|
TK.TCVN 7767:2007
|
1 mg/L
|
|
VII. HEAVY METAL AND OTHER METAL
|
|
69.
|
As
|
Ref. AOAC986.15
|
mg/L
|
|
70.
|
Hg(**)
|
Ref. AOAC986.15
|
mg/L
|
|
71.
|
Cd
|
AOAC 999.11
|
mg/L
|
|
72.
|
Pb
|
AOAC 999.11
|
mg/L
|
|
73.
|
Cu
|
AOAC 999.11
|
mg/L
|
|
74.
|
Ca
|
AOAC 969.23
|
mg/L
|
|
75.
|
Se
|
Ref. AOAC986.15
|
mg/L
|
|
76.
|
Fe
|
AOAC 999.11
|
mg/L
|
|
77.
|
Na
|
AOAC 969.23
|
mg/L
|
|
78.
|
Zn
|
AOAC 999.11
|
mg/L
|
|
79.
|
Sb
|
Ref. AOAC986.15
|
mg/L
|
|
80.
|
Borat
|
Ref. 3390/2000/QĐ-BYT
|
mg/L
|
|
81.
|
P2O5
|
Ref. EPA method 200.7
|
mg/L
|
|
VIII. PLANT PROTECTION DRUG RESIDUES
|
|
83.
|
Clo plant protection drug residues
|
TK.AOAC 2007.01 (LCMSMS)
|
-
|
|
|
2,4'-DDD
|
0.05mg/l
|
|
|
4,4'-DDE
|
0.05mg/l
|
|
|
2,4'-DDE
|
0.05mg/l
|
|
|
Alpha-Lindan
|
0.05mg/l
|
|
|
Gamma-Lindan
|
0.05mg/l
|
|
|
Beta-Lindan
|
0.05mg/l
|
|
|
Isodrin
|
0.05mg/l
|
|
|
Aldrin
|
0.05mg/l
|
|
|
Dieldrin
|
0.05mg/l
|
|
|
Hexachloro-Benzene
|
0.05mg/l
|
|
|
Heptachlor
|
0.05mg/l
|
|
|
Heptachlor epoxide
|
0.05mg/l
|
|
|
Endosulfan I
|
0.05mg/l
|
|
85.
|
Phosphor Pesticide
|
TK.AOAC 2007.01 (LCMSMS)
|
-
|
|
|
Fenthion
|
0.05mg/l
|
|
|
Diazinon
|
0.05mg/l
|
|
|
Parathion Methyl
|
0.05mg/l
|
|
|
Malathion
|
0.05mg/l
|
|
|
Chlorpyrifos
|
0.05mg/l
|
|
|
Parathion ethyl
|
0.05mg/l
|
|
|
Bromophos methyl
|
0.05mg/l
|
|
|
Bromophos ethyl
|
0.05mg/l
|
|
|
Ethion
|
0.05mg/l
|
|
86.
|
Chrysanthemum Pesticide
|
TK.AOAC 2007.01 (LCMSMS)
|
0.05mg/l
|
|
|
Cypermethrin
|
0.05mg/l
|
|
|
Deltamethrin
|
0.05mg/l
|
|
|
Permethrin
|
0.05mg/l
|
|
|
Fenvalerate
|
0.05mg/l
|
|
|
Resmethrine
|
0.05mg/l
|
|
|
Fenthropathrine
|
0.05mg/l
|
|
87.
|
Carbamate Pesticide
|
TK.AOAC 2007.01 (LCMSMS)
|
|
|
|
Isoprocarb
|
0.01mg/l
|
|
|
Aldicarb sulfone
|
0.01mg/l
|
|
|
Aldicarb
|
0.01mg/l
|
|
|
Aldicarb sulfoxide
|
0.01mg/l
|
|
|
Propoxur
|
0.01mg/l
|
|
|
Carbofuran
|
0.01mg/l
|
|
|
Carbaryl
|
0.01mg/l
|
|
|
Methomyl
|
0.01mg/l
|
|
|
Oxamyl
|
0.01mg/l
|
|
|
Thiodicarb
|
0.01mg/l
|
|
|
Methiocarb
|
0.01mg/l
|
|
|
Fenobucarb
|
0.01mg/l
|
|
|
Propoxur
|
0.01mg/l
|
|
|
Carbofuran-3-Hydroxy
|
0.01mg/l
|
|
IX. MYCOTOXIN
|
|
88.
|
Aflatoxin Tổng(**)
|
TK.AOAC 991.31 (LC/MS/MS)
|
1.0µg/l
|
|
89.
|
Aflatoxin/chất (B1, B2, G1, G2)(**)
|
TK.AOAC 991.31(LC/MS/MS)
|
1.0µg/l
|
|
90.
|
Ochratoxin A(**)
|
TK. AOAC 2000.09(LC/MS/MS)
|
1.0µg/l
|
|
91.
|
Deoxynivalenol (DON)(**)
|
TK.AOAC 986.18 (LC/MS/MS)
|
100µg/l
|
|
92.
|
Zearalenone(**)
|
TK .Analytical Chimica Acta 487, p137-143 (LC/MS/MS)
|
1.0µg/l
|
|
X. MICROBIOLOGY
|
|
A.
|
TPC
|
ISO 4833-1:2013
|
CFU/G
|
|
93
|
Enterobacteriaceae
|
ISO 21528-2:2004
|
CFU/G
|
|
94
|
Coliform
|
ISO 4832:2006
|
CFU/G
|
|
95
|
E. coli
|
ISO 16649-2:2001
|
CFU/G
|
|
96
|
E. coli
|
ISO 7251:2005
|
MPN/G; /G
|
|
97
|
Staphylococcus positive coagulase
|
ISO 6888-1:1999
|
CFU/G
|
|
98
|
Staphylococcus aureus
|
ISO 6888-1:1999
|
CFU/G
|
|
99
|
Salmonella
|
ISO 6579:2002
|
/25G
|
|
100
|
Vibrio parahaemolyticus
|
ISO 21872-1:2007
|
/25G
|
|
101
|
Vibrio cholerae
|
ISO 21872-1:2007
|
/25G
|
|
102
|
Listeria monocytogenes
|
ISO 11290-1:1996/ Amd.1:2004
|
/25G
|
|
103
|
Total yeast - mould
|
ISO 21527-1&2: 2008
|
CFU/G
|
|
104
|
Clostridium perfringens
|
ISO 7937:2004
|
CFU/G
|
|
105
|
Spores of sulfite-reducing anaerobes (Clostridia)
|
ISO 15213:2003
|
CFU/G
|