Quality testing competence in animal feed (04/03/2015)

No

CRITERIA

TEST METHOD

LOD (Unit)

I. ORGANOLEPTIC AND PHYSICAL MECHANICS 

1.       

Organoleptic (appearance, odor, flavor)

Organoleptic

-

2.       

Impurities (sand)

AOAC 920.46 (2011)

0.02%

II.  QUALITY INGREDIENTS

 

 

 

3.       

Độ ẩm

TCVN 4326 :2001

% wt

4.       

Protein thô

TCVN 4328-1:2007

% wt

5.       

Protein Tiêu hóa(**)

AOAC 971.09 (2011)

0.05%

6.       

Protein tan trong KOH(**)

Kjeldahl method

0.05%

7.       

Nito bay hơi (TVN)

TCVN 3706-1990

mg/100g

8.       

Nito bazo bay hơi (TVBN)

FAO 14/8, p.140, 1986

mg/100g

9.       

Carbohydrate

Calculate (Included testing Carbohydrate, Fat, Protein),
 Food Composition

Kcal/100g

10.  

Tinh bột(**)

FAO, 14/7, 1986

0.02%

11.  

Béo

FAO 14/7 p. 212, 1986

%wt

12.  

Hàm lượng xơ thô

TCVN 4329: 2007

%wt

13.  

Độ acid(**)

TCVN 4589:1988

0.05 ml NaOH 1N/100g

14.  

Tro tổng

AOAC 942.05 (2011)

0.02%

 

Tro tổng

TCVN 4327:2007

0.01%

15.  

Tro không an trong HCl

TCVN 4327:2008

0.01%

16.  

Hàm lượng chất khô(**)

AOAC 930.15 (2011)

0.02%

17.  

Muối (NaCl)

AOAC 937.09 (2011)

0.01%

III. OTHER INGREDIENTS

18.  

Acid amine (gồm 20 acid

amine)(**)

TK.EZ : faast (LCMSMS)

10 mg/kg

 

Glycine

10 mg/kg

 

Alanine

 

 

Serine

 

 

Proline

 

 

Valine

 

 

Threonine

 

 

Methionine

 

 

Trans-4-hydroxy-proline

 

 

Arginine

 

 

Aspartic acid

 

 

Glutamic acid

 

 

Cysteine

 

 

Lysine

 

 

Histidine

 

 

Tyrosine

 

 

Cystine

 

 

Leucine _ Isoleucine

 

 

Phenylalamine

 

19

Saturated fatty acid(**)

TK.AOAC 996.06 for food,              TK.AOAC 969.33 for oil (GC/FID)

20mg/kg

20.  

Monounsaturated fatty

acid(**)

TK.AOAC 996.06 for food,                        TK.AOAC 969.33 for oil (GC/FID)

20mg/kg

21.  

Polyunsaturated fatty

acid(**)

TK.AOAC 996.06 for food,                        TK.AOAC 969.33 for oil (GC/FID)

20mg/kg

22.  

Trans fat(**)

TK.AOAC 996.06 for food,                      TK.AOAC 969.33 for oil (GC/FID)

20mg/kg

23.  

Omega 3(**)

TK.AOAC 996.06 for food                TK.AOAC 969.33 for oil (GC/FID)  

20mg/kg

24.  

Omega 6(**)

TK.AOAC 996.06 for food,                        TK.AOAC 969.33 for oil (GC/FID)

20mg/kg

25.  

Omega 9(**)

TK.AOAC 996.06 for food,                       TK.AOAC 969.33 for oil (GC/FID)

20mg/kg

26.  

DHA(**)

TK.AOAC 996.06 for food,                        TK.AOAC 969.33 for oil (GC/FID)

20mg/kg

27.  

Cholesterol(**)

TK.AOAC 970.51 (LCMSMS)

1.0mg/kg

28.  

Taurin(**)

TK. AOAC 997.05 -2002 (LCMSMS)

2.0mg/kg

29.  

Urê(**)

TK. Appilication Note SSI – AP – LCMS 0277 – Shimadzu (LCMSMS)

5.0mg/kg

IV. NITRIT AND NITRAT RESIDUES

30.  

Nitrit (NO2-)(**)

TK.TCVN 7767:2007

1 mg/Kg

31.  

Nitrat (NO3-)(**)

TK.TCVN 7767:2007

1 mg/Kg

V. HEAVY METAL AND OTHER METALS

 

 

 

32.  

Arsen (As) 

BSEN 15510 - 2007

0.01 mg/Kg

33.  

Thủy ngân (Hg)(**)

AOAC 974.14 (2011)

0.01 mg/Kg

34.  

Cadimi (Cd) 

AOAC 968.08

0.005 mg/Kg

35.  

Chì (Pb) 

AOAC 968.08

0.01 mg/Kg

36.  

Đồng (Cu) 

AOAC 968.08

0.2 mg/Kg

37.  

Canxi (Ca) 

AOAC 968.08

0.5 mg/Kg

38.  

Selen (Se)

BSEN 15510 - 2007

0.01 mg/Kg

39.  

Kali (K) 

AOAC 968.08

0.5 mg/Kg

40.  

Magie (Mg) 

AOAC 968.08

0.5 mg/Kg

41.  

Mangan (Mn)

AOAC 968.08

0.5 mg/Kg

42.  

Sắt (Fe) 

AOAC 968.08

0.5 mg/Kg

43.  

Natri (Na) 

AOAC 968.08

0.5 mg/Kg

44.  

Antimo (Sb)

BSEN 15510 - 2007

0.01 mg/Kg

45.  

Kẽm (Zn) 

AOAC 968.08

0.5  mg/Kg

46.  

Arsen (As) 

BSEN 15510 - 2007

0.01 mg/Kg

VI. ANTIBIOTIC RESIDUES

 

 

 

47.  

Chloramphenicol

LC/MS/MS

0.1mg/kg

48.  

Fluoro-quinolones

LC/MS/MS

 

 

Ciprofloxacin

10.0mg/kg

 

Enrofloxacin

10.0mg/kg

 

Difloxacin

10.0mg/kg

 

Sarafloxacin

10.0mg/kg

 

Norfloxacin

10.0mg/kg

 

Danofloxacin

10.0mg/kg

 

Ofloxacin

10.0mg/kg

 

Flumequine

100mg/kg

 

Oxolinic acid

100mg/kg

49.  

Malachite green

LC/MS/MS

1.0mg/kg

50.  

Leucomalachite green

LC/MS/MS

1.0mg/kg

51.  

Nitrofuran và các dẫn

xuấ(4 dẫn xuất)

LC/MS/MS

1.0mg/kg

 

AOZ (3-amino-2-

oxazolidinone)

1.0mg/kg

 

AMOZ ( 3-amino-5-

morpholinomethyl-

1,3-oxazolidin-2-one)

1.0mg/kg

 

AHD (1-aminohydrantoin)

1.0mg/kg

 

SEM ( Semicarbazide)

1.0mg/kg

52.  

Crystal Violet

LC/MS/MS

1.0mg/kg

53.  

Leucocrystal Violet

1.0mg/kg

54.  

Họ Tetracyline

-

 

Tetracyclin

100mg/kg

 

Chlortetracyclin

100mg/kg

 

Oxytetracyclin

LC/MS/MS

100mg/kg

55.  

Florfenicol

100mg/kg

56.  

Họ Sulfonamides

 

 

Sulfamethoxazole

50.0mg/kg

 

Sulfadicine

50.0mg/kg

 

Sulfadiazine

LC/MS/MS

50.0mg/kg

 

Sulfathiazole

50.0mg/kg

 

Sulfamidine

50.0mg/kg

57.  

Trifluralin

0.2mg/kg

58.  

Ethoxyquin

10.0mg/kg

59.  

Beta-Lactamines

TK.Analytical Chimica Acta 520 ( 2004), p14-32, 590 – 3722 EN, Agilent  (LCMSMS)

 

 

Amipicillin

100mg/kg

 

Amoxycillin

100mg/kg

 

Benxylpenicillin

100mg/kg

60.  

Streptomycin(**)

TK. CLG – AMG -1.03, USDA (LCMSMS)

100mg/kg

61.  

Spiramycin(**)

TK. CLG – AMG -1.03, USDA (LCMSMS)

50.0mg/kg

62.  

Gentamycin(**)

TK. CLG – AMG -1.03, USDA (LCMSMS)

50.0mg/kg

63.  

Tylosin(**)

TK. CLG – AMG -1.03, USDA (LCMSMS)

50.0mg/kg

64.  

Lincomycin(**)

TK. CLG – AMG -1.03, USDA (LCMSMS)

50.0mg/kg

65.  

Họ Nitroimidazole(**)

TK. CLG – AMG -1.03, USDA (LCMSMS)

 

 

Ronidazole(**)

10.0mg/kg

 

Omidazole(**)

10.0mg/kg

 

Metronidazole(**)

10.0mg/kg

 

Ipronidazole(**)

10.0mg/kg

 

Dimetridazole(**)

10.0mg/kg

 

Tinidazole(**)

10.0mg/kg

VII. PLANT PROTECTION DRUG RESIDUES

 

 

 

66.  

Carbamate plant protection drug residues

TK.AOAC 2007.01 (LCMSMS)

 

 

Isoprocarb

0.01mg/kg

 

Aldicarb sulfone

0.01mg/kg

 

Aldicarb

0.01mg/kg

 

Aldicarb sulfoxide

0.01mg/kg

 

Propoxur

0.01mg/kg

 

Carbofuran

0.01mg/kg

 

Carbaryl

0.01mg/kg

 

Methomyl

0.01mg/kg

 

Oxamyl

0.01mg/kg

 

Thiodicarb

0.01mg/kg

 

Methiocarb

0.01mg/kg

 

Fenobucarb

0.01mg/kg

 

Propoxur

0.01mg/kg

 

Carbofuran-3-Hydroxy

0.01mg/kg

67.  

Clo plant protection drug residues

TK.AOAC 2007.01 (GCMS)

-

 

2,4'-DDD

0.1mg/kg

 

4,4'-DDD

0.1mg/kg

 

2,4'-DDE

0.1mg/kg

 

4,4'-DDE

0.1mg/kg

 

2,4'-DDT

0.1mg/kg

 

4,4'-DDT

0.1mg/kg

 

Alpha-Lindan

0.1mg/kg

 

Gamma-Lindan

0.1mg/kg

 

Beta-Lindan

0.1mg/kg

 

Isodrin

0.1mg/kg

 

Aldrin

0.1mg/kg

 

Dieldrin

0.1mg/kg

 

Endrin

0.1mg/kg

 

Hexachloro-Benzene

0.1mg/kg

 

Heptachlor

0.1mg/kg

 

Heptachlor epoxide

0.1mg/kg

 

Endosulfan I

0.1mg/kg

 

Endosulfan II

0.1mg/kg

68.  

Phosphor plant protection drug residues

TK.AOAC 2007.01 (GCMS)

-

 

Diazinon

0.1mg/kg

 

Parathion Methyl

0.1mg/kg

 

Malathion

0.1mg/kg

 

Chlorpyrifos

0.1mg/kg

 

Parathion ethyl

0.1mg/kg

 

Bromophos methyl

0.1mg/kg

 

Bromophos ethyl

0.1mg/kg

 

Ethion

0.1mg/kg

69.  

Chrysanthemum plant protection drug residues

TK.AOAC 2007.01 (GCMS)

-

 

Cypermethrin

0.1mg/kg

 

Deltamethrin

0.1mg/kg

 

Permethrin

0.1mg/kg

 

Fenvalerate

0.1mg/kg

 

Resmethrine

0.1mg/kg

 

Fenthropathrine

0.1mg/kg

VIII.  VITAMIN

 

 

 

70.  

Vitamin A(**)

TK.AOAC 992.06:2011 (HPLC.UV)

0.1mg/kg

71.  

Vitamin D3(**)

TK.AOAC 992.06:2011 (HPLC.UV)

0.1mg/kg

72.  

Vitamin E(**)

TK.AOAC 992.06:2011 (HPLC.UV)

0.1mg/kg

73.  

Vitamin C

Ref Journal of Chromatography A UHPLC-DAD

1.0mg/kg

74.  

Vitamin B1

Ref Journal of Chromatography A UHPLC-DAD

0.1mg/kg

75.  

Vitamin B2

Ref Journal of Chromatography A UHPLC-DAD

0.1mg/kg

76.  

Vitamin B3

(nicotinamide)

Ref Journal of Chromatography A UHPLC-DAD

0.1mg/kg

77.  

Vitamin B5

(acid pantothenic)

Ref Journal of Chromatography A UHPLC-DAD

0.1mg/kg

78.  

Vitamin B6

Ref Journal of Chromatography A UHPLC-DAD

0.1mg/kg

79.  

Vitamin B9

(floic acid)

Ref Journal of Chromatography A UHPLC-DAD

0.1mg/kg

80.  

Vitamin B12

Ref Journal of Chromatography A UHPLC-DAD

0.1mg/kg

81.  

Biotin(**)

TK.AOAC 985.33:2011 (HPLC-UV)

0.1mg/kg

IX. ADDITIVES

 

 

 

82.  

Acid citric (E330)

Ref Megazyme International Ireland 2012
UHPLC-DAD

20.0mg/kg

83.  

Acid Tartaric (E334)(**)

TK. US EPA method 300.00(IC)

20.0mg/kg

84.  

Acid malic (E296)(**)

TK. US EPA method 300.00(IC)

20.0mg/kg

85.  

Acid fumaric (E297)(**)

TK. US EPA method 300.00(IC)

20.0mg/kg

86.  

Acid lactic (E270)(**)

TK. US EPA method 300.00(IC)

20.0mg/kg

87.  

Acid ascorbic

/Natri ascorbate

Ref Megazyme International Ireland 2012
UHPLC-DAD

1.0mg/kg

88.  

Aicd propionic(**)

TK. US EPA method 300.00(IC)

20.0mg/kg

89.  

Aicd fomic(**)

TK. US EPA method 300.00(IC)

20.0mg/kg

90.  

Acid acetic

/Natri acetate(**)

TK. US EPA method 300.00(IC)

20.0mg/kg

91.  

Natri benzoate

/ Acid benzoic

Ref Journal of chromatography A, 1073(2005) 393 – 397
UHPLC-DAD

10mg/kg

92.  

Kali sorabte/ Acid sorbic

Ref Megazyme International Ireland 2012
UHPLC-DAD

10mg/kg

93.  

Benzoyl peroxyd(**)

(HPLC/UV)

10.0mg/kg

94.  

Paraben(**)

TK. AOAC 983.16 (HPLC/UV)

 

 

Butylparaben

(Butyl-4-hydroxy

benzoate)(**)

10.0mg/kg

 

Ethylparaben

(Ethyl-4-hydroxy

benzoate)(**)

10.0mg/kg

 

Methylparaben

(Methyl-4-hydroxy

benzoate)(**)

10.0mg/kg

 

Propylparaben

(Propyl-4-hydroxy

benzoate)(**)

10.0mg/kg

 

Heptylparaben

(Heptyl-4-hydroxy

benzoate)(**)

10.0mg/kg

95.  

Alpha-Tocopherol(**)

TK : AOAC 992.06 (HPLC/UV)

0.1mg/kg

96.  

BHA (Butylated

hydroxyanisol)(**)

TK : AOAC 983.15 (HPLC/UV)

5.0mg/kg

97.  

BHT (Butylated

hydroxytoluene)(**)

TK : AOAC 983.15 (HPLC/UV)

5.0mg/kg

98.  

TBHQ (Tert-Butyl

hydroquinone)(**)

TK : AOAC 983.15 (HPLC/UV)

5.0mg/kg

X. GROWTH STIMULATION_ HORMON

 

 

 

99.  

Beta agonist

LC/MS/MS

 

 

Salbutamol

LC/MS/MS

1.0mg/kg

 

Clenbuterol

LC/MS/MS

1.0mg/kg

 

Ractopamine

LC/MS/MS

1.0mg/kg

100.          

Dexamethasone(**)

TK. Journal of chromatoghaphy B, volume 862, issue 1-2, p119 -124 (LCMSMS)

0.30µg/kg

101.          

Hormons(**)

TK. CLG – AMG -1.03, USDA (LCMSMS)

 

 

Progesterol(**)

50.0µg/kg

 

Estradiol(**)

50.0µg/kg

 

Testosterone(**)

50.0µg/kg

 

Dietylstylbestrole(**)

50.0µg/kg

XI. TOXIN

 

 

 

102.          

Aflatoxin Tổng(**)

TK.AOAC 991.31 (LC/MS/MS)

1.0µg/kg

103.          

Aflatoxin/chất

(B1, B2, G1, G2)(**)

TK.AOAC 991.31(LC/MS/MS)

1.0µg/kg

104.          

Ochratoxin A(**)

TK. AOAC 2000.09(LC/MS/MS)

1.0µg/kg

105.          

Deoxynivalenol

(DON)(**)

TK.AOAC 986.18 (LC/MS/MS)

100µg/kg

106.          

Zearalenone(**)

TK .Analytical Chimica Acta 487, p137-143 (LC/MS/MS)

1.0µg/kg

107.          

Melamine(**)

TK. FDA 4396  (LC/MS/MS)

100µg/kg

XII. MICROBIOLOGY

 

 

 

108.          

Enzyme lipase(**)

PP định phân acid béo

_

109.          

Aspergillus(**)

Định danh nấm mốc, ISO 215272 : 2008

 

110.          

Xác định vi khuẩn

khử sulfit phát triển

trong điều kiện kỵ khí(*)

ISO 15213: 2003

10 CFU/g

111.          

Phát hiện Vibrio cholerae - 

Phương pháp phát hiện

Vibrio spp,có khả năng

gây bệnh đường ruột (*)

TCVN 7905-1:2008, (ISO 21872-1:2007 E)

/25g

 Note:

TCVN : Vietnam Standards                           

AOAC: Association of Official Analytical Chemist (USA)                            

FAO: Food and Agriculture Organization                        

(**) Criteria  is performed by subcontractor

TK: Normative references

Criteria are not included in this table will agree the development and application with customers about method

Released time:

5 working days. In special case, depending on the requirements of customers will be agreed later.

Vinacert willing to perform the services and return the results on holidays as agreement with customer.

Representative sample volume: 800 grams

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