Quality testing competence and analysis fee in vegetables, fruits and vegetables, fruits, cereals, agricultural products (04/03/2015)

No

CRITERIA

TEST METHODS

LOD

I. ORGANOLEPTIC

1.        

Apperance (**)

Cảm quan

-

2.        

Odor (**)

Cảm quan

-

3.        

Flavor (**)

Cảm quan

-

4.        

Tỉ lệ cái, tịnh (**)

TCVN 4414:1987

0.02%

II. QUALITY INGREDIENT

5.        

Độ ẩm

FAO, 14/7, 1986

0.02%

6.        

Đường tổng(**)

TCVN 4594:1988

0.02%

7.        

Độ chua(**)

TCVN 4589:1988

0.05 ml NaOH 1N/100g

8.        

Carbohydrate

TCVN 4594:1988

0.05%

9.        

Xơ thô

TK.TCVN 5103:1990

0.02%

10.     

Tinh bột(**)

FAO, 14/7, 1986

0.02%

11.     

Muối (NaCl)

AOAC 937.09 (2011)

0.01%

12.     

Chỉ số Peroxyt(**)

TCVN 6121:2010

0.2 meq/Kg

13.     

Chỉ số acid(**)

TCVN 6127:2010

0.1 mg KOH/g

14.     

Protein thô

FAO, 14/7, 1986

0.05%

15.     

Tro tổng

FAO, 14/7, 1986

0.02%

16.     

Béo tổng

FAO, 14/7, 1986

0.10%

17.     

Béo bão hòa(**)

TK.AOAC 966.17 (2011)

0.10%

18.     

Xơ tiêu hóa (Dietary Fiber)(**)

AOAC 985.29 (2011)

0.02%

19.     

Tro không tan trong HCl

AOAC 920.46 (2011)

0.02%

20.     

Phospho tổng số

AOAC 995.11 (2011)

0.01%

21.     

Năng lượng (tính từ béo, đạm, carbohydrate)

Bảng NUTRITION FACTS

-

 

NUTRITION FACTS

Serving Size                            …………

 

 

Serving Per Container             …………

 

 

Amount Per Serving              . …………

 

 

Calories                                   …………                                     Calories from fat       …………

 

 

% Daily Value(*) 

Total Fat                                 …………                                                                        …………

 

 

Saturated Fat                          …………                                                                         …………

 

 

Trans fat                                  …………                                                                        …………

 

 

Cholesterol                              …………                                                                        …………

 

 

Sodium                                     …………                                                                      ………… 

 

Total carbohydrate                    …………                                                                      …………

 

 

Dietary fiber                               …………                                                                     …………

 

 

Sugar                                         …………                                                                      …………

 

 

Protein                                       …………                                                                       …………

 

 

Vitamin A                               …………                       Vitamin C                 …………

 

 

Calcium                                   …………                       Iron                          …………

 

 

(*)Percent Daily Value are based on 2,000 calories diet. Your daily values may be higher or lower
 depending on your calorie needs: 

                                            Calories                    2,000                       s 2,5000

 

 

Total Fat                         less than                      65g                            80g

 

 

Saturated Fat                less than              20g                           25g

 

 

Cholesterol                    less than               300mg                       300 mg

 

 

Sodium                           less than               2400mg                     2400 mg

 

 

Total carbohydrate         less than               300g                          375g

 

 

Fiber                               less than                   25g                            30g                         -

 

 

Calories per gram: 

Fat 9                                         Carbohydrate 4                                   Protein 4

 

 

 

No

CRITERIA

TEST METHOD

LOD

III. VITAMIN

22.     

Vitamin A(**)

TK.AOAC 992.06:2011 (HPLC.UV)

0.1mg/kg

23.     

Vitamin D3(**)

TK.AOAC 992.06:2011 (HPLC.UV)

0.1mg/kg

24.     

Vitamin E(**)

TK.AOAC 992.06:2011 (HPLC.UV)

0.1mg/kg

25.     

Vitamin C

Ref Journal of Chromatography A UHPLC-DAD

1.0mg/kg

26.     

Vitamin B1

Ref Journal of Chromatography A UHPLC-DAD

0.1mg/kg

27.     

Vitamin B2

Ref Journal of Chromatography A UHPLC-DAD

0.1mg/kg

28.     

Vitamin B3 (Nicotinamide)

Ref Journal of Chromatography A UHPLC-DAD

0.1mg/kg

29.     

Vitamin B5 (Acid pantothenic)

Ref Journal of Chromatography A UHPLC-DAD

0.1mg/kg

30.     

Vitamin B6

Ref Journal of Chromatography A UHPLC-DAD

0.1mg/kg

31.     

Vitamin B9 (Floic acid)

Ref Journal of Chromatography A UHPLC-DAD

0.1mg/kg

32.     

Vitamin B12

Ref Journal of Chromatography A UHPLC-DAD

0.1mg/kg

33.     

Biotin(**)

TK.AOAC 985.33:2011 (HPLC-UV)

0.1mg/kg

IV.       PRESERVATION

34.     

Sunfuadioxite (SO2)

AOAC 962.16

2(mg/kg)

35.     

Natri benzoate / Acid benzoic

Ref Journal of chromatography A, 1073(2005) 393 – 397
UHPLC-DAD

10.0mg/l

36.     

Kali sorabte/ Acid sorbic

Ref Journal of Chromatography A
UHPLC-DAD

10.0mg/l

37.     

Aicd propionic(**)

TK. US EPA method 300.00(IC)

20.0mg/kg

38.     

Aicd fomic(**)

TK. US EPA method 300.00(IC)

20.0mg/kg

39.     

Acid acetic / Natri acetate(**)

TK. US EPA method 300.00(IC)

20.0mg/l

V.          ADDITIVES

40.     

BHA (Butylated hydroxyanisol)(**)

TK : AOAC 983.15 (HPLC/UV)

5.0mg/kg

41.     

BHT (Butylated hydroxytoluene)(**)

TK : AOAC 983.15 (HPLC/UV)

5.0mg/kg

42.     

TBHQ (Tert-Butyl hydroquinone)(**)

TK : AOAC 983.15 (HPLC/UV)

5.0mg/kg

43.     

Acid citric (E330)

Ref Megazyme International Ireland 2012
UHPLC-DAD

20.0mg/kg

44.     

Acid lactic (E270)(**)

TK. US EPA method 300.00(IC)

20.0mg/kg

45.     

Acid ascorbic / Natri ascorbate

Ref Journal of Chromatography A
UHPLC-DAD

1.0mg/kg

46.     

Benzoyl peroxyd(**)

(HPLC/UV)

10.0mg/kg

47.     

Melamine(**)

TK. FDA 4396  (LC/MS/MS)

100µg/kg

VI. NITRIT AND NITRAT RESIDUES

48.     

Nitrit (NO2-)(**)

TK.TCVN 7767:2007

1 mg/Kg

49.     

Nitrat (NO3-)(**)

TK.TCVN 7767:2007

1 mg/Kg

VII.  HEAVY METAL AND OTHER METAL

50.     

Arsen (As) 

AOAC 986.15 (2011)

0.01 mg/Kg

51.     

Thủy ngân (Hg)(**)

AOAC 974.14 (2011)

0.01 mg/Kg

52.     

Cadimi (Cd) 

AOAC 999.11 (2011)

0.005 mg/Kg

53.     

Chì (Pb) 

AOAC 999.11 (2011)

0.01 mg/Kg

54.     

Đồng (Cu) 

AOAC 999.11 (2011)

0.2 mg/Kg

55.     

Canxi (Ca) 

AOAC 999.23

0.5 mg/Kg

56.     

Selen (Se)

AOAC 986.15 (2011)

0.01 mg/Kg

57.     

Kali (K) 

AOAC 999.23

0.5 mg/Kg

58.     

Magie (Mg) 

AOAC 999.23

0.5 mg/Kg

59.     

Mangan (Mn)

AOAC 999.11 (2011)

0.5 mg/Kg

60.     

Sắt (Fe) 

AOAC 999.11 (2011)

0.5 mg/Kg

61.     

Natri (Na) 

AOAC 999.23

0.5 mg/Kg

62.     

Antimo (Sb)

TK.AOAC 986.15 (2011)

0.01 mg/Kg

63.     

Kẽm (Zn) 

AOAC 999.11 (2011)

0.5  mg/Kg

VIII. PLANT PROTECTION DRUG RESIDUES

64.     

Clo plant protection drug residues

TK.AOAC 970.52 (GCMS)

-

 

Alpha-Lindane

3.1mg/kg

 

Gamma-Lindane

3.2mg/kg

 

Beta-Lindane

3.2mg/kg

 

Eldrin

2.7mg/kg

 

2,4'-DDE

1.2mg/kg

 

4,4'-DDE

1.4mg/kg

 

Endosulfan I

3.3mg/kg

 

Endosulfan II

3.2mg/kg

 

2,4' DDD

2.8mg/kg

 

4,4’ DDD

1.2mg/kg

 

2,4’-DDT

1.5mg/kg

 

4,4’-DDT

1.5mg/kg

65.     

Phosphor plant protection drug residues

TK.AOAC 970.52 (LCMSMS)

_

 

Diazinon

1.5mg/kg

 

Parathion methyl

3.3mg/kg

 

Malathion

2.8mg/kg

 

Chlorpyrifos

1.0mg/kg

 

Parathion ethyl

3.3mg/kg

 

Bromophos methyl

3.3mg/kg

 

Bromophos ethyl

3.3mg/kg

 

Ethion

3.1mg/kg

66.     

Chrysanthemum plant protection drug residues

 

_

 

Fenthropathrine

10.0mg/kg

 

Resmethrine

10.0mg/kg

 

Permethrine 1

10.0mg/kg

 

Permethrine 2

10.0mg/kg

 

Cypermethrine 1

10.0mg/kg

 

Cypermethrine 2

10.0mg/kg

 

Cypermethrine 3

10.0mg/kg

 

Cypermethrine 4

10.0mg/kg

 

Fenvalerate 1

10.0mg/kg

 

Fenvalerate 2

15.0mg/kg

 

Deltamethrine

15.0mg/kg

67.     

Carbamate plant protection drug residues

 

0.5mg/kg

 

Isoprocarb

0.5mg/kg

 

Aldicarb sulfone

0.5mg/kg

 

Aldicarb

0.5mg/kg

 

Aldicarb sulfoxide

0.5mg/kg

 

Propoxur

0.5mg/kg

 

Carbofuran

0.5mg/kg

 

Carbaryl

0.5mg/kg

 

Methomyl

0.5mg/kg

 

Oxamyl

0.5mg/kg

 

Thiodicarb

0.5mg/kg

 

Methiocarb

0.5mg/kg

 

Fenobucarb

0.5mg/kg

 

Propoxur

0.5mg/kg

 

Carbofuran-3-Hydroxy

0.5mg/kg

68.     

2,4D(**)

TK.AOAC 2007.01 (LCMSMS)

10.0mg/kg

69.     

Abamectin(**)

TK.AOAC 2007.01 (LCMSMS)

10.0mg/kg

70.     

Acephate(**)

TK.AOAC 2007.01 (LCMSMS)

10.0mg/kg

71.     

Carbendazim (**)

TK.AOAC 2007.01 (LCMSMS)

10.0mg/kg

72.     

Chlorantraniliprole(**)

TK.AOAC 2007.01 (LCMSMS)

10.0mg/kg

73.     

Difenoconazole(**)

TK.AOAC 2007.01 (LCMSMS)

10.0mg/kg

74.     

Emamectine benzoate(**)

TK.AOAC 2007.01 (LCMSMS)

10.0mg/kg

75.     

Flusilazole(**)

TK.AOAC 2007.01 (LCMSMS)

10.0mg/kg

76.     

Imidacloprid(**)

TK.AOAC 2007.01 (LCMSMS)

10.0mg/kg

77.     

Indoxacarb(**)

TK.AOAC 2007.01 (LCMSMS)

10.0mg/kg

78.     

Paraquat(**)

TK.AOAC 2007.01 (LCMSMS)

10.0mg/kg

79.     

Pirimicarb(**)

TK.AOAC 2007.01 (LCMSMS)

10.0mg/kg

80.     

Propiconazole(**)

TK.AOAC 2007.01 (LCMSMS)

10.0mg/kg

81.     

Tebuconazole(**)

TK.AOAC 2007.01 (LCMSMS)

10.0mg/kg

82.     

Thiamethoxam(**)

TK.AOAC 2007.01 (LCMSMS)

10.0mg/kg

83.     

Azinphos-methyl(**)

TK.AOAC 2007.01 (GCMS)

100mg/kg

84.     

Bentazone(**)

TK.AOAC 2007.01 (GCMS)

100mg/kg

85.     

Diflubanzuron(**)

TK.AOAC 2007.01 (GCMS)

100mg/kg

86.     

Ethoprophos(**)

TK.AOAC 2007.01 (GCMS)

100mg/kg

87.     

Fenamiphos(**)

TK.AOAC 2007.01 (GCMS)

100mg/kg

88.     

Fenitrothion(**)

TK.AOAC 2007.01 (GCMS)

100mg/kg

89.     

Profenofos(**)

TK.AOAC 2007.01 (GCMS)

10mg/kg

90.     

Fludioxonil(**)

TK.AOAC 2007.01 (GCMS)

100mg/kg

91.     

Metalaxyl(**)

TK.AOAC 2007.01 (GCMS)

10mg/kg

92.     

Terbufos(**)

TK.AOAC 2007.01 (GCMS)

100mg/kg

93.     

Triazophos(**)

TK.AOAC 2007.01 (GCMS)

100mg/kg

94.     

Isoprothiolane(**)

TK.AOAC 2007.01 (GCMS)

1mg/kg

IX. MYCOTOXIN

95.     

Aflatoxin Tổng(**)

TK.AOAC 991.31 (LC/MS/MS)

1.0µg/kg

96.     

Aflatoxin/chất (B1, B2, G1, G2)(**)

TK.AOAC 991.31(LC/MS/MS)

1.0µg/kg

97.     

Ochratoxin A(**)

TK. AOAC 2000.09(LC/MS/MS)

1.0µg/kg

98.     

Deoxynivalenol (DON)(**)

TK.AOAC 986.18 (LC/MS/MS)

100µg/kg

99.     

Zearalenone(**)

TK .Analytical Chimica Acta 487, p137-143 (LC/MS/MS)

1.0µg/kg

100. 

Aflatoxin M1(**)

AOAC 986.16:2002 (HPLC-UV

0.01µg/kg

X. MICROBIOLOGY

A.    Cereal,  potato and bean products (flour, vermicelli, noodle, etcheat treatment before using)

101. 

Tổng số vi khuẩn hiếu khí (*)

TCVN 4884:2005, ISO 4833:2003

Dạng lỏng:1 CFU/mL,          Dạng khác:10 CFU/g

102. 

Coliforms(*) (CFU)

TCVN 6848:2007, ISO 4832:2007

Dạng lỏng:1 CFU/mL,          Dạng khác:10 CFU/g

103. 

Coliforms(*) (CFU)

AOAC 991.14:2011  ( Petrifilm)

Dạng lỏng:1 CFU/mL,          Dạng khác:10 CFU/g

104. 

E.coli(*) (CFU)

AOAC 991.14:2011 ( Petrifilm)

Dạng lỏng:1 CFU/mL,          Dạng khác:10 CFU/g

105. 

E.coli(*) (CFU)

TCVN 7924-2:2008, ISO 16649-2:2001

Dạng lỏng:1 CFU/mL,          Dạng khác:10 CFU/g

106. 

Staphylococcus aureus (*)

TCVN 4830-1:2005 (ISO 6888-1:2003)

Dạng lỏng:1 CFU/mL,          Dạng khác:10 CFU/g

107. 

Staphylococcus aureus(*)

AOAC 2003.07:2011 ( Petrifilm)

Dạng lỏng:1 CFU/mL,          Dạng khác:10 CFU/g

108. 

Clostridium perfringens(*)

TCVN 4991:2005(ISO 7937:2004)

Dạng lỏng:1 CFU/mL,          Dạng khác:10 CFU/g

109. 

Bacillus cereus(*)

TCVN 4992:2005, ISO 7932:2004

Dạng lỏng:1 CFU/mL,          Dạng khác:10 CFU/g

110. 

Nấm men-Nấm mốc(*)

TCVN 8275-1:2010, ISO 21527-1:2008 (dạng lỏng), TCVN 8275-2:2010 ISO 21527-2:2008 (dạng rắn)

Dạng lỏng:1 CFU/mL,          Dạng khác:10 CFU/g

B. Cereal,  potato and bean products (cake, flour, etc: used directly, not through heat treatment before using)

111. 

Tổng số vi khuẩn hiếu khí (*)

TCVN 4884:2005,ISO 4833:2003

Dạng lỏng:1 CFU/mL,          Dạng khác:10 CFU/g

112. 

Coliforms(*) (CFU)

TCVN 6848:2007, ISO 4832:2006

Dạng lỏng:1 CFU/mL,          Dạng khác:10 CFU/g

113. 

Coliforms(*) (CFU)

AOAC 991.14:2011  ( Petrifilm)

Dạng lỏng:1 CFU/mL,          Dạng khác:10 CFU/g

114. 

E.coli(*) (MPN)

TCVN 6846:2007, ISO 7251:2005

Dạng lỏng:1 CFU/mL,          Dạng khác:10 CFU/g

115. 

Staphylococcus aureus (*)

TCVN 4830-1:2005, ISO 6888-1:2003

Dạng lỏng:1 CFU/mL,          Dạng khác:10 CFU/g

116. 

Staphylococcus aureus(*)

AOAC 2003.07:2011 ( Petrifilm)

Dạng lỏng:1 CFU/mL,          Dạng khác:10 CFU/g

117. 

Clostridium perfringens(*)

TCVN 4991:2005,ISO 7937:2004

Dạng lỏng:1 CFU/mL,          Dạng khác:10 CFU/g

118. 

Bacillus cereus(*)

TCVN 4992:2005, ISO 7932:2004

Dạng lỏng:1 CFU/mL,          Dạng khác:10 CFU/g

119. 

Nấm men-Nấm mốc(*)

TCVN 8275-1:2010, ISO 21527-1:2008 (dạng lỏng), TCVN 8275-2:2010 ISO 21527-2:2008 (dạng rắn)

Dạng lỏng:1 CFU/mL,          Dạng khác:10 CFU/g

Note:

TCVN : Vietnam Standards                           

AOAC: Association of Official Analytical Chemist (USA)                            

FAO: Food and Agriculture Organization                        

(**) Criteria  is performed by subcontractor

TK: Normative references

Criteria are not included in this table will agree the development and application with customers about method

Released time:

5 working days. In special case, depending on the requirements of customers will be agreed later.

Vinacert willing to perform the services and return the results on holidays as agreement with customer.

Representative sample volume: 800 grams

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