Quality testing competence and analysis fee in milk samples and milk products (04/03/2015)

No

CRITERIA

TEST METHOD

LOD

I. ORGANOLEPTIC

1.       

Organoleptic (appearance, odor, flavor)

Organoleptic

-

2.       

Impurities (sand) (**)

AOAC 920.46 (2011)

0.02%

3.       

Density (**)

TCVN 7028:2009

-

II.  QUALITY INGREDIENT

4.       

pH(**)

TK.TCVN 7806:2007

-

5.       

Độ ẩm

FAO 14/7, p.205, 1986

%wt

6.       

Protein 

FAO 14/7, p.205, 1986

%wt

7.       

Béo

 FAO 14/8 p. 221-223, 1986

%wt

8.       

Đường(**)

TCVN 4594:1988

0.05%

9.       

Carbohydrate

Calculate (Included testing Carbohydrate, Fat, Protein),
 Food Composition

Kcal/100g

10.  

Xơ hòa tan(**)

AOAC 985.29 (2011)

0.02%

11.  

Độ acid(**)

TCVN 8079:2009 & AOAC 947.05 (2011)

0.05 ml NaOH 0.1N/10g

12.  

Độ acid (oT)(**)

TCVN 6509:1999

-

13.  

Chỉ số không hòa tan(**)

TCVN 6511:2007

-

14.  

Hàm lượng chất khô(**)

Ref. FAO 14/7

0.02%

15.  

Hàm lượng chất khô không chứa chất béo(**)

TCVN 7729:2007

0.02%

16.  

Tro tổng

TCVN 5105:2009 (AOAC 938.08)

0.02%

17.  

Tro không tan trong HCl

TCVN 5105:2009 (AOAC 938.08)

0.02%

18.  

P2O5

Ref. EPA method 200.7

 

19.  

Năng lượng (tính từ béo, đạm, carbohydrate)

Calculate (Included testing Carbohydrate, Fat, Protein),
 Food Composition

Kcal/100g

 

III.  NUTRITION FACTS TABLE  -  Total analysis fee: 2.650.000 (VNĐ)   

NUTRITION FACTS

 

 

Serving Size                   …………

 

 

Serving Per Container    …………

 

 

Amount Per Serving        …………

 

 

Calories                             …………                       Carlories from fat    …………

                                                                                   % Daily Value*

Total Fat                            …………                              …………

Saturated Fat                   …………                               …………

Transfat                            …………                              …………

Cholesterol                      …………                                …………

Sodium                             …………                               …………

Total carbohydrat           …………                                 …………

Dietary fiber                    …………                                …………

Sugars                               …………                               …………

Protein                              ………….                               …………

Vitamine A                        …………                          

Vitamine C                        …………

Calcium                             …………                         

 Iron                                   …………

*Percent Daily Value are base on 2,000 calories diet. Your daily values may be higher or lower depending on your calorie needs: 

 Calories                      2,000                      2,5000 

Total Fat                         less than                    65g                          80g

Saturated Fat                  less than                    20g                           25g

Cholesterol                     less than                    300mg                     300mg

Sodium                           less than                    2400mg                   2400mg

Total carbohydrat           less than                     300g                        375g

Fiber                               less than                     25g                          30g                         

Calories per gram

Fat 9                      Carbohydrat 4                                   Protein 4

 

No

CRITERIA

TEST METHOD

LOD

IV. NITRIT AND NITRAT RESIDUES

20.  

Nitrit (NO2-)(**)

TK.TCVN 7806:2007

1 mg/Kg

21.  

Nitrat (NO3-)(**)

TK.TCVN 7806:2007

1 mg/Kg

V.  HEAVY METAL AND OTHER METALS

22.  

Arsen (As) 

AOAC 986.15 (2011)

0.01 mg/Kg

23.  

Thủy ngân (Hg) (**)

AOAC 974.14 (2011) & TCVN 7993:2009

0.01 mg/Kg

24.  

Cadimi (Cd) 

AOAC 999.11 (2011)

0.005 mg/Kg

25.  

Chì (Pb) 

AOAC 999.11 (2011)

0.01 mg/Kg

26.  

Đồng (Cu) 

AOAC 999.11 (2011)

0.2 mg/Kg

27.  

Canxi (Ca) 

AOAC 999.23

0.5 mg/Kg

28.  

Selen (Se)

AOAC 986.15 (2011)

0.01 mg/Kg

29.  

Kali (K) 

AOAC 999.23

0.5 mg/Kg

30.  

Magie (Mg) 

AOAC 999.23

0.5 mg/Kg

31.  

Mangan (Mn)

AOAC 999.11 (2011)

0.5 mg/Kg

32.  

Sắt (Fe) 

AOAC 999.11 (2011)

0.5 mg/Kg

33.  

Natri (Na) 

AOAC 999.23

0.5 mg/Kg

34.  

Antimo (Sb)

TK.AOAC 986.15 (2011)

0.01 mg/Kg

35.  

Kẽm (Zn) 

AOAC 999.11 (2011)

0.5  mg/Kg

VI. OTHER INGREDIENTS

36.  

Acid amine (gồm 20 acid amine)(**)

TK.EZ : faast (LCMSMS)

10.0 mg/kg

 

Glycine(**)

10.0 mg/kg

 

Alanine(**)

 

 

Serine(**)

 

 

Proline(**)

 

 

Valine(**)

 

 

Threonine(**)

 

 

Methionine(**)

 

 

Trans-4-hydroxy-proline(**)

 

 

Arginine(**)

 

 

Aspartic acid(**)

 

 

Glutamic acid(**)

 

 

Cysteine(**)

 

 

Lysine(**)

 

 

Histidine(**)

 

 

Tyrosine(**)

 

 

Cystine(**)

 

 

Leucine _ Isoleucine(**)

 

 

Phenylalamine(**)

 

 

Saturated fatty acid(**)

TK.AOAC 996.06 for food  (GC/FID)

20mg/kg

38.  

Monounsaturated fatty acid(**)

TK.AOAC 996.06 for food (GC/FID)

20mg/kg

39.  

Polyunsaturated fatty acid(**)

TK.AOAC 996.06 for food (GC/FID)

20mg/kg

40.  

Trans fat(**)

TK.AOAC 996.06 for food (GC/FID)

20mg/kg

41.  

Omega 3(**)

TK.AOAC 996.06 for food (GC/FID)

20mg/kg

42.  

Omega 6(**)

TK.AOAC 996.06 for food (GC/FID)

20mg/kg

43.  

Omega 9(**)

TK.AOAC 996.06 for food (GC/FID)

20mg/kg

44.  

DHA(**)

TK.AOAC 996.06 for food (GC/FID)

20mg/kg

45.  

Cholesterol(**)

TK.AOAC 970.51 (LCMSMS)

1.0mg/kg

46.  

DEHP(**)

TK. AOAC 2000.01 (GCMS)

0.1mg/kg

47.  

DINP(**)

TK. AOAC 2000.01 (GCMS)

0.1mg/kg

VII. ANTIBIOTIC RESIDUES 

48.  

Họ Tetracyline

TK. AOAC 995.09 (LCMSMS)

 

 

Tetracyclin

100.0mg/kg

 

Chlortetracyclin

100.0mg/kg

 

Oxytetracyclin

100.0mg/kg

49.  

Họ Sulfonamide

TK. Journal of Chro A 1177 (LCMSMS)

 

 

Sulfamethoxazole

20.0mg/kg

 

Sulfadicine

20.0mg/kg

 

Sulfadiazine

20.0mg/kg

 

Sulfathiazole

20.0mg/kg

 

Sulfamidine

20.0mg/kg

50.  

Beta-Lactamine(**)

TK.Analytical Chimica Acta 520 ( 2004), p14-32, 590 – 3722 EN, Agilent  (LCMSMS)

 

 

Amipicillin(**)

1.0mg/kg

 

Amoxycillin(**)

1.0mg/kg

 

Benzylpenicillin(**)

1.0mg/kg

51.  

Streptomycin(**)

TK. CLG – AMG -1.03, USDA (LCMSMS)

100mg/kg

52.  

Spiramycin(**)

TK. CLG – AMG -1.03, USDA (LCMSMS)

50.0mg/kg

53.  

Gentamycin(**)

TK. CLG – AMG -1.03, USDA (LCMSMS)

50.0mg/kg

54.  

Tylosin(**)

TK. CLG – AMG -1.03, USDA (LCMSMS)

10.0mg/kg

55.  

Lincomycin(**)

TK. CLG – AMG -1.03, USDA (LCMSMS)

10.0mg/kg

56.  

Họ Nitroimidazole(**)

TK. CLG – AMG -1.03, USDA (LCMSMS)

 

 

Ronidazole(**)

1.0mg/kg

 

Omidazole(**)

1.0mg/kg

 

Metronidazole(**)

1.0mg/kg

 

Ipronidazole(**)

1.0mg/kg

 

Dimetridazole(**)

1.0mg/kg

 

Tinidazole(**)

50.0mg/kg

VIII.  VITAMIN 

57.  

Vitamin A(**)

TK.AOAC 992.06:2011 (HPLC.UV)

0.1mg/kg

58.  

Vitamin D3(**)

TK.AOAC 992.06:2011 (HPLC.UV)

0.1mg/kg

59.  

Vitamin K

Ref Journal of Chromatography A
UHPLC-DAD

0.1mg/kg

60.  

Vitamin E(**)

TK.AOAC 992.06:2011 (HPLC.UV)

0.1mg/kg

61.  

Vitamin C

Ref Journal of Chromatography A
UHPLC-DAD

1.0mg/kg

62.  

Vitamin B1

Ref Journal of Chromatography A
UHPLC-DAD

0.1mg/kg

63.  

Vitamin B2

Ref Journal of Chromatography A
UHPLC-DAD

0.1mg/kg

64.  

Vitamin B3 (Nicotinamide)

Ref Journal of Chromatography A
UHPLC-DAD

0.1mg/kg

65.  

Vitamin B5 (Acid pantothenic)

Ref Journal of Chromatography A
UHPLC-DAD

0.1mg/kg

66.  

Vitamin B6

Ref Journal of Chromatography A
UHPLC-DAD

0.1mg/kg

67.  

Vitamin B9 (Folic acid)

Ref Journal of Chromatography A
UHPLC-DAD

0.1mg/kg

68.  

Vitamin B12

Ref Journal of Chromatography A
UHPLC-DAD

0.1mg/kg

69.  

Biotin(**)

TK.AOAC 985.33:2011 (HPLC-UV)

0.1mg/kg

IX.  QUANTITIES OF PLANT PROTECTION DRUG RESIDUES

70.  

Carbamate plant protection drug residues

TK.AOAC 2007.01 (LCMSMS)

 

 

Isoprocarb

0.01mg/kg

 

Aldicarb sulfone

0.01mg/kg

 

Aldicarb (*)

0.005mg/kg

 

Aldicarb sulfoxide (*0

0.005mg/kg

 

Propoxur

0.01mg/kg

 

Carbofuran (*)

0.02mg/kg

 

Carbaryl (*)

0.02mg/kg

 

Methomyl (*)

0.01mg/kg

 

Oxamyl (*)

0.01mg/kg

 

Thiodicarb

0.01mg/kg

 

Methiocarb (*)

0.005mg/kg

 

Fenobucarb

0.01mg/kg

 

Propoxur

0.01mg/kg

 

Carbofuran-3-Hydroxy

0.01mg/kg

71.  

Clo plant protection drug residues

TK.AOAC 2007.01 (GCMS)

-

 

2,4'-DDD

0.01mg/kg

 

4,4'-DDD

0.01mg/kg

 

2,4'-DDE

0.01mg/kg

 

4,4'-DDE

0.01mg/kg

 

2,4'-DDT

0.01mg/kg

 

4,4'-DDT

0.01mg/kg

 

Alpha-Lindan

0.005mg/kg

 

Gamma-Lindan

0.005mg/kg

 

Beta-Lindan

0.005mg/kg

 

Isodrin

0.003mg/kg

 

Aldrin

0.003mg/kg

 

Dieldrin

0.003mg/kg

 

Endrin

0.003mg/kg

 

Hexachloro-Benzene

0.003mg/kg

 

Heptachlor

0.003mg/kg

 

Heptachlor epoxide

0.003mg/kg

 

Endosulfan I

0.01mg/kg

 

Endosulfan II

0.01mg/kg

72.  

Phosphor plant protection drug residues

TK.AOAC 2007.01 (LCMSMS)

-

 

Diazinon

0.01mg/kg

 

Parathion Methyl

0.01mg/kg

 

Malathion

0.01mg/kg

 

Chlorpyrifos

0.01mg/kg

 

Parathion ethyl

0.01mg/kg

 

Bromophos methyl

0.01mg/kg

 

Bromophos ethyl

0.01mg/kg

 

Ethion

0.01mg/kg

73.  

Chrysanthemum plant protection drug residues

TK.AOAC 2007.01 (GCMS)

-

 

Cypermethrin

0.025mg/kg

 

Deltamethrin

0.025mg/kg

 

Permethrin

0.05mg/kg

 

Fenvalerate

0.05mg/kg

 

Resmethrine

0.05mg/kg

 

Fenthropathrine

0.05mg/kg

74.  

Abamectine(**)

AOAC 2007.01 (LCMSMS)

0.01mg/kg

75.  

Acephate (**)

AOAC 2007.01 (LCMSMS)

0.01mg/kg

76.  

Carbendazim (**)

AOAC 2007.01 (LCMSMS)

0.005mg/kg

77.  

Chlorantraniliprole(**)

AOAC 2007.01 (LCMSMS)