|
No
|
CRITERIA
|
TEST METHOD
|
LOD
|
|
IV. NITRIT AND NITRAT RESIDUES
|
|
20.
|
Nitrit (NO2-)(**)
|
TK.TCVN 7806:2007
|
1 mg/Kg
|
|
21.
|
Nitrat (NO3-)(**)
|
TK.TCVN 7806:2007
|
1 mg/Kg
|
|
V. HEAVY METAL AND OTHER METALS
|
|
22.
|
Arsen (As)
|
AOAC 986.15 (2011)
|
0.01 mg/Kg
|
|
23.
|
Thủy ngân (Hg) (**)
|
AOAC 974.14 (2011) & TCVN 7993:2009
|
0.01 mg/Kg
|
|
24.
|
Cadimi (Cd)
|
AOAC 999.11 (2011)
|
0.005 mg/Kg
|
|
25.
|
Chì (Pb)
|
AOAC 999.11 (2011)
|
0.01 mg/Kg
|
|
26.
|
Đồng (Cu)
|
AOAC 999.11 (2011)
|
0.2 mg/Kg
|
|
27.
|
Canxi (Ca)
|
AOAC 999.23
|
0.5 mg/Kg
|
|
28.
|
Selen (Se)
|
AOAC 986.15 (2011)
|
0.01 mg/Kg
|
|
29.
|
Kali (K)
|
AOAC 999.23
|
0.5 mg/Kg
|
|
30.
|
Magie (Mg)
|
AOAC 999.23
|
0.5 mg/Kg
|
|
31.
|
Mangan (Mn)
|
AOAC 999.11 (2011)
|
0.5 mg/Kg
|
|
32.
|
Sắt (Fe)
|
AOAC 999.11 (2011)
|
0.5 mg/Kg
|
|
33.
|
Natri (Na)
|
AOAC 999.23
|
0.5 mg/Kg
|
|
34.
|
Antimo (Sb)
|
TK.AOAC 986.15 (2011)
|
0.01 mg/Kg
|
|
35.
|
Kẽm (Zn)
|
AOAC 999.11 (2011)
|
0.5 mg/Kg
|
|
VI. OTHER INGREDIENTS
|
|
36.
|
Acid amine (gồm 20 acid amine)(**)
|
TK.EZ : faast (LCMSMS)
|
10.0 mg/kg
|
|
|
Glycine(**)
|
10.0 mg/kg
|
|
|
Alanine(**)
|
|
|
|
Serine(**)
|
|
|
|
Proline(**)
|
|
|
|
Valine(**)
|
|
|
|
Threonine(**)
|
|
|
|
Methionine(**)
|
|
|
|
Trans-4-hydroxy-proline(**)
|
|
|
|
Arginine(**)
|
|
|
|
Aspartic acid(**)
|
|
|
|
Glutamic acid(**)
|
|
|
|
Cysteine(**)
|
|
|
|
Lysine(**)
|
|
|
|
Histidine(**)
|
|
|
|
Tyrosine(**)
|
|
|
|
Cystine(**)
|
|
|
|
Leucine _ Isoleucine(**)
|
|
|
|
Phenylalamine(**)
|
|
|
|
Saturated fatty acid(**)
|
TK.AOAC 996.06 for food (GC/FID)
|
20mg/kg
|
|
38.
|
Monounsaturated fatty acid(**)
|
TK.AOAC 996.06 for food (GC/FID)
|
20mg/kg
|
|
39.
|
Polyunsaturated fatty acid(**)
|
TK.AOAC 996.06 for food (GC/FID)
|
20mg/kg
|
|
40.
|
Trans fat(**)
|
TK.AOAC 996.06 for food (GC/FID)
|
20mg/kg
|
|
41.
|
Omega 3(**)
|
TK.AOAC 996.06 for food (GC/FID)
|
20mg/kg
|
|
42.
|
Omega 6(**)
|
TK.AOAC 996.06 for food (GC/FID)
|
20mg/kg
|
|
43.
|
Omega 9(**)
|
TK.AOAC 996.06 for food (GC/FID)
|
20mg/kg
|
|
44.
|
DHA(**)
|
TK.AOAC 996.06 for food (GC/FID)
|
20mg/kg
|
|
45.
|
Cholesterol(**)
|
TK.AOAC 970.51 (LCMSMS)
|
1.0mg/kg
|
|
46.
|
DEHP(**)
|
TK. AOAC 2000.01 (GCMS)
|
0.1mg/kg
|
|
47.
|
DINP(**)
|
TK. AOAC 2000.01 (GCMS)
|
0.1mg/kg
|
|
VII. ANTIBIOTIC RESIDUES
|
|
48.
|
Họ Tetracyline
|
TK. AOAC 995.09 (LCMSMS)
|
|
|
|
Tetracyclin
|
100.0mg/kg
|
|
|
Chlortetracyclin
|
100.0mg/kg
|
|
|
Oxytetracyclin
|
100.0mg/kg
|
|
49.
|
Họ Sulfonamide
|
TK. Journal of Chro A 1177 (LCMSMS)
|
|
|
|
Sulfamethoxazole
|
20.0mg/kg
|
|
|
Sulfadicine
|
20.0mg/kg
|
|
|
Sulfadiazine
|
20.0mg/kg
|
|
|
Sulfathiazole
|
20.0mg/kg
|
|
|
Sulfamidine
|
20.0mg/kg
|
|
50.
|
Beta-Lactamine(**)
|
TK.Analytical Chimica Acta 520 ( 2004), p14-32, 590 – 3722 EN, Agilent (LCMSMS)
|
|
|
|
Amipicillin(**)
|
1.0mg/kg
|
|
|
Amoxycillin(**)
|
1.0mg/kg
|
|
|
Benzylpenicillin(**)
|
1.0mg/kg
|
|
51.
|
Streptomycin(**)
|
TK. CLG – AMG -1.03, USDA (LCMSMS)
|
100mg/kg
|
|
52.
|
Spiramycin(**)
|
TK. CLG – AMG -1.03, USDA (LCMSMS)
|
50.0mg/kg
|
|
53.
|
Gentamycin(**)
|
TK. CLG – AMG -1.03, USDA (LCMSMS)
|
50.0mg/kg
|
|
54.
|
Tylosin(**)
|
TK. CLG – AMG -1.03, USDA (LCMSMS)
|
10.0mg/kg
|
|
55.
|
Lincomycin(**)
|
TK. CLG – AMG -1.03, USDA (LCMSMS)
|
10.0mg/kg
|
|
56.
|
Họ Nitroimidazole(**)
|
TK. CLG – AMG -1.03, USDA (LCMSMS)
|
|
|
|
Ronidazole(**)
|
1.0mg/kg
|
|
|
Omidazole(**)
|
1.0mg/kg
|
|
|
Metronidazole(**)
|
1.0mg/kg
|
|
|
Ipronidazole(**)
|
1.0mg/kg
|
|
|
Dimetridazole(**)
|
1.0mg/kg
|
|
|
Tinidazole(**)
|
50.0mg/kg
|
|
VIII. VITAMIN
|
|
57.
|
Vitamin A(**)
|
TK.AOAC 992.06:2011 (HPLC.UV)
|
0.1mg/kg
|
|
58.
|
Vitamin D3(**)
|
TK.AOAC 992.06:2011 (HPLC.UV)
|
0.1mg/kg
|
|
59.
|
Vitamin K
|
Ref Journal of Chromatography A
UHPLC-DAD
|
0.1mg/kg
|
|
60.
|
Vitamin E(**)
|
TK.AOAC 992.06:2011 (HPLC.UV)
|
0.1mg/kg
|
|
61.
|
Vitamin C
|
Ref Journal of Chromatography A
UHPLC-DAD
|
1.0mg/kg
|
|
62.
|
Vitamin B1
|
Ref Journal of Chromatography A
UHPLC-DAD
|
0.1mg/kg
|
|
63.
|
Vitamin B2
|
Ref Journal of Chromatography A
UHPLC-DAD
|
0.1mg/kg
|
|
64.
|
Vitamin B3 (Nicotinamide)
|
Ref Journal of Chromatography A
UHPLC-DAD
|
0.1mg/kg
|
|
65.
|
Vitamin B5 (Acid pantothenic)
|
Ref Journal of Chromatography A
UHPLC-DAD
|
0.1mg/kg
|
|
66.
|
Vitamin B6
|
Ref Journal of Chromatography A
UHPLC-DAD
|
0.1mg/kg
|
|
67.
|
Vitamin B9 (Folic acid)
|
Ref Journal of Chromatography A
UHPLC-DAD
|
0.1mg/kg
|
|
68.
|
Vitamin B12
|
Ref Journal of Chromatography A
UHPLC-DAD
|
0.1mg/kg
|
|
69.
|
Biotin(**)
|
TK.AOAC 985.33:2011 (HPLC-UV)
|
0.1mg/kg
|
|
IX. QUANTITIES OF PLANT PROTECTION DRUG RESIDUES
|
|
70.
|
Carbamate plant protection drug residues
|
TK.AOAC 2007.01 (LCMSMS)
|
|
|
|
Isoprocarb
|
0.01mg/kg
|
|
|
Aldicarb sulfone
|
0.01mg/kg
|
|
|
Aldicarb (*)
|
0.005mg/kg
|
|
|
Aldicarb sulfoxide (*0
|
0.005mg/kg
|
|
|
Propoxur
|
0.01mg/kg
|
|
|
Carbofuran (*)
|
0.02mg/kg
|
|
|
Carbaryl (*)
|
0.02mg/kg
|
|
|
Methomyl (*)
|
0.01mg/kg
|
|
|
Oxamyl (*)
|
0.01mg/kg
|
|
|
Thiodicarb
|
0.01mg/kg
|
|
|
Methiocarb (*)
|
0.005mg/kg
|
|
|
Fenobucarb
|
0.01mg/kg
|
|
|
Propoxur
|
0.01mg/kg
|
|
|
Carbofuran-3-Hydroxy
|
0.01mg/kg
|
|
71.
|
Clo plant protection drug residues
|
TK.AOAC 2007.01 (GCMS)
|
-
|
|
|
2,4'-DDD
|
0.01mg/kg
|
|
|
4,4'-DDD
|
0.01mg/kg
|
|
|
2,4'-DDE
|
0.01mg/kg
|
|
|
4,4'-DDE
|
0.01mg/kg
|
|
|
2,4'-DDT
|
0.01mg/kg
|
|
|
4,4'-DDT
|
0.01mg/kg
|
|
|
Alpha-Lindan
|
0.005mg/kg
|
|
|
Gamma-Lindan
|
0.005mg/kg
|
|
|
Beta-Lindan
|
0.005mg/kg
|
|
|
Isodrin
|
0.003mg/kg
|
|
|
Aldrin
|
0.003mg/kg
|
|
|
Dieldrin
|
0.003mg/kg
|
|
|
Endrin
|
0.003mg/kg
|
|
|
Hexachloro-Benzene
|
0.003mg/kg
|
|
|
Heptachlor
|
0.003mg/kg
|
|
|
Heptachlor epoxide
|
0.003mg/kg
|
|
|
Endosulfan I
|
0.01mg/kg
|
|
|
Endosulfan II
|
0.01mg/kg
|
|
72.
|
Phosphor plant protection drug residues
|
TK.AOAC 2007.01 (LCMSMS)
|
-
|
|
|
Diazinon
|
0.01mg/kg
|
|
|
Parathion Methyl
|
0.01mg/kg
|
|
|
Malathion
|
0.01mg/kg
|
|
|
Chlorpyrifos
|
0.01mg/kg
|
|
|
Parathion ethyl
|
0.01mg/kg
|
|
|
Bromophos methyl
|
0.01mg/kg
|
|
|
Bromophos ethyl
|
0.01mg/kg
|
|
|
Ethion
|
0.01mg/kg
|
|
73.
|
Chrysanthemum plant protection drug residues
|
TK.AOAC 2007.01 (GCMS)
|
-
|
|
|
Cypermethrin
|
0.025mg/kg
|
|
|
Deltamethrin
|
0.025mg/kg
|
|
|
Permethrin
|
0.05mg/kg
|
|
|
Fenvalerate
|
0.05mg/kg
|
|
|
Resmethrine
|
0.05mg/kg
|
|
|
Fenthropathrine
|
0.05mg/kg
|
|
74.
|
Abamectine(**)
|
AOAC 2007.01 (LCMSMS)
|
0.01mg/kg
|
|
75.
|
Acephate (**)
|
AOAC 2007.01 (LCMSMS)
|
|