Quality testing competence and analysis fee in biscuits, jam, candies (04/03/2015)

No

CRITERIA

TEST METHOD

LOD

I. ORGANOLEPTIC

1.        

Appearance

Organoleptic

-

2.        

Odor

Organoleptic

-

3.        

Flavor

Organoleptic

-

II. QUALITY INGREDIENT

1.        

pH(**)

TK.TCVN 7806:2007

-

2.        

Độ ẩm

FAO 14/7, p.205, 1986

%wt

3.        

Đường tổng(**)

TCVN 4594:1988

0.02%

4.        

Carbohydrate

Calculate (Included testing Carbohydrate, Fat, Protein),
 Food Composition

Kcal/100g

5.        

Protein thô

 FAO 14/8 p. 221-223, 1986

%wt

6.        

Béo tổng

 FAO 14/8 p. 221-223, 1986

%wt

7.        

Béo bão hòa(**)

TK.AOAC 966.17 (2011)

0.10%

8.        

Xơ thô

TCVN 4329: 2007

%wt

9.        

Xơ tiêu hóa (Dietary Fiber)(**)

AOAC 985.29 (2011)

0.02%

10.     

Độ chua(**)

TCVN 4589:1988

0.05 ml NaOH 1N/100g

11.     

Tro tổng

TCVN 5105:2009 (AOAC 938.08)

0.02%

12.     

Tro không tan trong HCl

TCVN 5105:2009 (AOAC 938.08)

0.02%

13.     

Phospho tổng số

AOAC 995.11 (2011)

0.00%

14.     

Năng lượng (tính từ béo, đạm, carbohydrate)

Calculate (Included testing Carbohydrate, Fat, Protein),
 Food Composition

-

 

NUTRITION FACTS

 

 

Serving Size                            …………

 

 

Serving Per Container             …………

 

 

Amount Per Serving               …………

 

 

Calories                                   …………                      Calories from fat       …………

 

 

% Daily Value(*)

 

 

Total Fat                                 …………                                                         …………

 

Saturated Fat                          …………                                                         …………

Trans fat                                  …………                                                         …………

Cholesterol                              …………                                                         …………

 

Sodium                                   …………                                                         …………

Total carbohydrate                  …………                                                         …………

Dietary fiber                           …………                                                         …………

Sugars                                     …………                                                         …………

Protein                                    …………                                                         …………

Vitamin A                               …………                       Vitamin C                 …………

Calcium                                   …………                        Iron                          …………

(*)Percent Daily Value are based on 2,000 calories diet. Your daily values may be higher or lower depending on your calorie needs:

                                            Calories                    2,000                       s 2,5000 

Total Fat                         less than                    65g                            80g 

Saturated Fat                less than                    20g                           25g

Cholesterol                    less than                    300mg                       300 mg 

Sodium                           less than                    2400mg                     2400 mg

Total carbohydrate         less than                    300g                          375g

Fiber                               less than                    25g                            30g                         

Calories per gram:

Fat 9                                         Carbohydrate 4                                   Protein 4 

 

No

CRITERIA

TEST METHOD

LOD (Unit)

III. VITAMIN 

15.     

Vitamin A(**)

TK.AOAC 992.06:2011 (HPLC.UV)

0.1mg/kg

16.     

Vitamin D3(**)

TK.AOAC 992.06:2011 (HPLC.UV)

0.1mg/kg

17.     

Vitamin E(**)

TK.AOAC 992.06:2011 (HPLC.UV)

0.1mg/kg

18.     

Vitamin C

Ref Journal of Chromatography A
UHPLC-DAD

1.0mg/kg

19.     

Vitamin B1

Ref Journal of Chromatography A
UHPLC-DAD

0.1mg/kg

20.     

Vitamin B2

Ref Journal of Chromatography A
UHPLC-DAD

0.1mg/kg

21.     

Vitamin B3 (Nicotinamide)

Ref Journal of Chromatography A
UHPLC-DAD

0.1mg/kg

22.     

Vitamin B5 (Acid pantothenic)

Ref Journal of Chromatography A
UHPLC-DAD

0.1mg/kg

23.     

Vitamin B6

Ref Journal of Chromatography A
UHPLC-DAD

0.1mg/kg

24.     

Vitamin B9 (Floic acid)

Ref Journal of Chromatography A
UHPLC-DAD

0.1mg/kg

25.     

Vitamin B12

Ref Journal of Chromatography A
UHPLC-DAD

0.1mg/kg

26.     

Biotin(**)

TK.AOAC 985.33:2011 (HPLC-UV)

0.1mg/kg

IV. NITRIT AND NITRAT RESIDUES

27.     

Nitrit (NO2-)(**)

TK.TCVN 7767:2007

1 mg/Kg

28.     

Nitrat (NO3-)(**)

TK.TCVN 7767:2007

1 mg/Kg

V. HEAVY METAL AND OTHER METALS

29.     

Arsen (As) 

AOAC 986.15 (2011)

0.01 mg/Kg

30.     

Thủy ngân (Hg)(**)

AOAC 974.14 (2011)

0.01 mg/Kg

31.     

Cadimi (Cd) 

AOAC 999.11 (2011)

0.005 mg/Kg

32.     

Chì (Pb) 

AOAC 999.11 (2011)

0.01 mg/Kg

33.     

Đồng (Cu) 

AOAC 999.11 (2011)

0.2 mg/Kg

34.     

Canxi (Ca)

AOAC 999.23

 

35.     

Selen (Se)

AOAC 986.15 (2011)

0.01 mg/Kg

36.     

Kali (K)

AOAC 999.23

 

37.     

Magie (Mg)

AOAC 999.23

 

38.     

Mangan (Mn)

AOAC 999.11 (2011)

0.5 mg/Kg

39.     

Sắt (Fe) 

AOAC 999.11 (2011)

0.5 mg/Kg

40.     

Natri (Na)

AOAC 999.23

 

41.     

Antimo (Sb)

TK.AOAC 986.15 (2011)

0.01 mg/Kg

42.     

Kẽm (Zn) 

AOAC 999.11 (2011)

0.5  mg/Kg

VI. OTHER INGREDIENTS

43.     

Acid amine (IN 20 acid amine)(**)

TK.EZ : faast (LCMSMS)

10.0 mg/kg

 

Glycine(**)

10.0 mg/kg

 

Alanine(**)

 

 

Serine(**)

 

 

Proline(**)

 

 

Valine(**)

 

 

Threonine(**)

 

 

Methionine(**)

 

 

Trans-4-hydroxy-proline(**)

 

 

Arginine(**)

 

 

Aspartic acid(**)

 

 

Glutamic acid(**)

 

 

Cysteine(**)

 

 

Lysine(**)

 

 

Histidine(**)

 

 

Tyrosine(**)

 

 

Cystine(**)

 

 

Leucine _ Isoleucine(**)

 

 

Phenylalamine(**)

 

 

Saturated fatty acid(**)

TK.AOAC 996.06 for food,TK.AOAC 969.33 for oil (GC/FID)

20mg/kg

45.     

Monounsaturated fatty acid(**)

TK.AOAC 996.06 for food, TK.AOAC 969.33 for oil (GC/FID)

20mg/kg

46.     

Polyunsaturated fatty acid(**)

TK.AOAC 996.06 for food, TK.AOAC 969.33 for oil (GC/FID)

20mg/kg

47.     

Trans fat(**)

TK.AOAC 996.06 for food, TK.AOAC 969.33 for oil (GC/FID)

20mg/kg

48.     

Omega 3(**)

TK.AOAC 996.06 for food, TK.AOAC 969.33 for oil (GC/FID)

20mg/kg

49.     

Omega 6(**)

TK.AOAC 996.06 for food, TK.AOAC 969.33 for oil (GC/FID)

20mg/kg

50.     

Omega 9(**)

TK.AOAC 996.06 for food, TK.AOAC 969.33 for oil (GC/FID)

20mg/kg

51.     

DHA(**)

TK.AOAC 996.06 for food, TK.AOAC 969.33 for oil (GC/FID)

20mg/kg

52.     

Cholesterol(**)

TK.AOAC 970.51 (LCMSMS)

1.0mg/kg

53.     

DEHP(**)

TK. AOAC 2000.01 (GCMS)

0.1mg/l

54.     

DINP(**)

TK. AOAC 2000.01 (GCMS)

0.1mg/l

55.     

Melamine(**)

TK. FDA 4396  (LC/MS/MS)

50µg/kg

VII. ADDITIVES

56.     

Monosodium Glutamate(**)

TK. EZ : faast (LCMSMS)

10.0mg/kg

57.     

Disodium Isosinate(**)

TK : HPLC Application Note 820435 (HPLC/UV)

5.0mg/kg

58.     

Disodium Guanylate(**)

TK : HPLC Application Note 820435 (HPLC/UV)

5.0mg/kg

59.     

Natri benzoate / Acid benzoic

Ref Journal of chromatography A, 1073(2005) 393 – 397
UHPLC-DAD

10.0mg/l

60.     

Kali sorabte/ Acid sorbic

Ref Journal of Chromatography A
UHPLC-DAD

10.0mg/l

61.     

Aicd propionic(**)

TK. US EPA method 300.00(IC)

20.0mg/kg

62.     

Aicd fomic(**)

TK. US EPA method 300.00(IC)

20.0mg/kg

63.     

Acid acetic / Natri acetate(**)

TK. US EPA method 300.00(IC)

20.0mg/l

64.     

Benzoyl peroxyd(**)

(HPLC/UV)

10.0mg/kg

65.     

Paraben(**)

TK. AOAC 983.16 (HPLC/UV)

 

66.     

Butylparaben (Butyl-4-hydroxybenzoate)(**)

TK. AOAC 983.16 (HPLC/UV)

10.0mg/kg

 

Ethylparaben (Ethyl-4-hydroxybenzoate)(**)

10.0mg/kg

 

Methylparaben (Methyl-4-hydroxybenzoate)(**)

10.0mg/kg

 

Propylparaben (Propyl-4-hydroxybenzoate)(**)

10.0mg/kg

 

Heptylparaben (Heptyl-4-hydroxybenzoate)(**)

10.0mg/kg

67.     

Acid citric (E330)

Ref Megazyme International Ireland 2012
UHPLC-DAD

20.0mg/kg

68.     

Acid Tartaric (E334)(**)

TK. US EPA method 300.00(IC)

20.0mg/kg

69.     

Acid malic (E296)(**)

TK. US EPA method 300.00(IC)

20.0mg/kg

70.     

Acid fumaric (E297)(**)

TK. US EPA method 300.00(IC)

20.0mg/kg

71.     

Acid lactic (E270)(**)

TK. US EPA method 300.00(IC)

20.0mg/kg

72.     

Acid ascorbic / Natri ascorbate

Ref Journal of Chromatography A
UHPLC-DAD

1.0mg/kg

73.     

Alpha-Tocopherol(**)

TK : AOAC 992.06 (HPLC/UV)

0.1mg/kg

74.     

BHA (Butylated hydroxyanisol)(**)

TK : AOAC 983.15 (HPLC/UV)

5.0mg/kg

75.     

BHT (Butylated hydroxytoluene)(**)

TK : AOAC 983.15 (HPLC/UV)

5.0mg/kg

76.     

TBHQ (Tert-Butyl hydroquinone)(**)

TK : AOAC 983.15 (HPLC/UV)

5.0mg/kg

77.     

Beta-caroten(**)

TK : AOAC 992.06 (HPLC/UV)

0.1mg/l

78.     

Curcumin(**)

(HPLC/UV)

10.0mg/kg

79.     

Orange II(**)

TK : LGC/GC/2007/005,Analysis of illegal Dyes in chilli Powder by LC-UV (HPLC/UV

0.1mg/kg

80.     

Parared(**)

TK : LGC/GC/2007/005 Analysis of illegal Dyes in chilli Powder by LC-UV (HPLC/UV

0.1mg/kg

81.     

Ponceau 4R(**)

TK : LGC/GC/2007/005 Analysis of illegal Dyes in chilli Powder by LC-UV (HPLC/UV

10.0mg/kg

82.     

Rhodamine B(**)

TK : Method No PV 2072, OSHA, USD (HPLC/UV)

0.1mg/kg

83.     

Riboflavin(**)

TK : AOAC 992.06 (HPLC/UV)

0.1mg/kg

84.     

Sudan(**)

TK : AOAC International Workshop " Food to Dyes For" (HPLC/UV)

0.1mg/kg

85.     

Sudan I(**)

0.1mg/kg

 

Sudan II(**)

0.1mg/kg

 

Sudan III(**)

0.1mg/kg

 

Sudan IV(**)

0.1mg/kg

86.     

Sunset yellow(**)

TK : JFDA Vol 14, No3, 2006, P284 – 291 (HPLC/UV)

10.0mg/kg

87.     

Tartazine(**)

TK : JFDA Vol 14, No3, 2006, P284 – 291 (HPLC/UV)

10.0mg/kg

VIII. PLANT PROTECTION DRUG RESIDUES

88.     

Carbamate plant protection drug residues

TK.AOAC 2007.01 (LCMSMS)

 

 

Isoprocarb

0.01mg/kg

 

Aldicarb sulfone

0.01mg/kg

 

Aldicarb

0.01mg/kg

 

Aldicarb sulfoxide

0.01mg/kg

 

Propoxur

0.01mg/kg

 

Carbofuran

0.01mg/kg

 

Carbaryl

0.01mg/kg

 

Methomyl

0.01mg/kg

 

Oxamyl

0.01mg/kg

 

Thiodicarb

0.01mg/kg

 

Methiocarb

0.01mg/kg

 

Fenobucarb

0.01mg/kg

 

Propoxur

0.01mg/kg

 

Carbofuran-3-Hydroxy

0.01mg/kg

89.     

Clo plant protection drug residues

TK.AOAC 2007.01 (GCMS)

-

 

2,4'-DDD

0.05mg/kg

 

4,4'-DDE

0.05mg/kg

 

2,4'-DDE

0.05mg/kg

 

Alpha-Lindan

0.05mg/kg

 

Gamma-Lindan

0.05mg/kg

 

Beta-Lindan

0.05mg/kg

 

Isodrin

0.05mg/kg

 

Aldrin

0.05mg/kg

 

Dieldrin

0.05mg/kg

 

Hexachloro-Benzene

0.05mg/kg

 

Heptachlor

0.05mg/kg

 

Heptachlor epoxide

0.05mg/kg

 

Endosulfan I

0.05mg/kg

90.     

Phosphor plant protection drug residues

TK.AOAC 2007.01 (GCMS)

0.05mg/kg

 

Fenthion

0.05mg/kg

 

Diazinon

0.05mg/kg

 

Parathion Methyl

0.05mg/kg

 

Malathion

0.05mg/kg

 

Chlorpyrifos

0.05mg/kg

 

Parathion ethyl

0.05mg/kg

 

Bromophos methyl

0.05mg/kg

 

Bromophos ethyl

0.05mg/kg

 

Ethion

0.05mg/kg

91.     

Chrysanthemum plant protection drug residues

TK.AOAC 2007.01 (GCMS)

0.05mg/kg

 

Cypermethrin

0.05mg/kg

 

Deltamethrin

0.05mg/kg

 

Permethrin

0.05mg/kg

 

Fenvalerate

0.05mg/kg

 

Resmethrine

0.05mg/kg

 

Fenthropathrine

0.05mg/kg

IX. MYCOTOXIN

92.     

Aflatoxin Tổng(**)

TK.AOAC 991.31(LC/MS/MS)

1.0µg/kg

93.     

Aflatoxin/chất (B1, B2, G1, G2)(**)

TK.AOAC 991.31(LC/MS/MS)

1.0µg/kg

94.     

Ochratoxin A(**)

AOAC 2000.09(LC/MS/MS)

1.0µg/kg

95.     

Deoxynivalenol (DON)(**)

TK.AOAC 986.18 (LC/MS/MS)

50µg/kg

96.     

Zearalenone(**)

TK .Analytical Chimica Acta 487, p137-143 (LC/MS/MS)

1.0µg/kg

X. MICROBIOLOGY

97.     

Tổng số vi khuẩn hiếu khí (*)

TCVN 4884:2005, ISO 4833:2003

Dạng lỏng:1 CFU/mL,      Dạng khác:10 CFU/g

98.     

Coliforms(*)(CFU)

TCVN 6848:2006, ISO 4832:2007

Dạng lỏng:1 CFU/mL,      Dạng khác:10 CFU/g

99.     

Coliforms(*)(CFU)

AOAC 991.14:2011 (Petrifilm)

Dạng lỏng:1 CFU/mL,      Dạng khác:10 CFU/g

100. 

E.coli(*) (CFU)

AOAC 991.14:2011( Petrifilm)

Dạng lỏng:1 CFU/mL,      Dạng khác:10 CFU/g

101. 

E.coli(*) (CFU)

TCVN 7924-2:2008, ISO 16649-2:2001

Dạng lỏng:1 CFU/mL,      Dạng khác:10 CFU/g

102. 

Staphylococcus aureus (*)

TCVN 4830-1:2005, (ISO 6888-1:2003)

Dạng lỏng:1 CFU/mL,      Dạng khác:10 CFU/g

103. 

Staphylococcus aureus(*)

AOAC 2003.07:2011 (Petrifilm)

Dạng lỏng:1 CFU/mL,      Dạng khác:10 CFU/g

104. 

Clostridium perfringens(*)

TCVN 4991:2005 (ISO 7937:2004)

Dạng lỏng:1 CFU/mL,      Dạng khác:10 CFU/g

105. 

Bacillus cereus(*)

TCVN 4992:2005, ISO 7932:2004

Dạng lỏng:1 CFU/mL,      Dạng khác:10 CFU/g

106. 

Nấm men-Nấm mốc(*)

TCVN 8275-2:2010, ISO 21527-2:2008 (dạng rắn)

10 CFU/g

Note:

TCVN : Vietnam Standards                           

AOAC: Association of Official Analytical Chemist (USA)                            

FAO: Food and Agriculture Organization                        

(**) Criteria  is performed by subcontractor

TK: Normative references

Criteria are not included in this table will agree the development and application with customers about method

Released time:

5 working days. In special case, depending on the requirements of customers will be agreed later.

Vinacert willing to perform the services and return the results on holidays as agreement with customer.

Representative sample volume: 800 grams

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