|
No
|
CRITERIA
|
TEST METHOD
|
LOD
|
|
I. ORGANOLEPTIC AND PHYSICAL MECHANICS
|
|
1.
|
Apperance
|
Organoleptic
|
-
|
|
2.
|
Odor
|
Organoleptic
|
-
|
|
3.
|
Flavor
|
Organoleptic
|
-
|
|
4.
|
Impurities (Sand) (**)
|
|
-
|
|
II. QUALITY INGREDIENT
|
|
5.
|
pH(**)
|
TCVN 6492:2011
|
-
|
|
6.
|
Hàm lượng chất khô
|
FAO, 14/7, 1986
|
0.02 g/100mL
|
|
7.
|
Đường(**)
|
TCVN 4594:1988
|
0.05 g/100mL
|
|
8.
|
Carbohydrate
|
TCVN 4594:1988
|
0.05 g/100mL
|
|
9.
|
Protein thô
|
FAO, 14/7, 1986
|
0.05 g/100mL
|
|
10.
|
Béo
|
FAO, 14/7, 1986
|
0.1 g/100mL
|
|
11.
|
Muối
|
AOAC 937.09 (2011)
|
0.005 g/100mL
|
|
12.
|
Độ cồn(**)
|
Cồn kế
|
-
|
|
13.
|
Ethanol(**)
|
TK. AOAC 972.10 (GC/FID)
|
-
|
|
14.
|
Độ acid(**)
|
TCVN 5564:2009
|
0.05 ml NaOH 1N/100mL
|
|
III. OTHER INGREDIENT
|
|
15.
|
Aceton(**)
|
TK. AOAC 972.10 (GC/MS)
|
-
|
|
16.
|
Biogenic amine(**)
|
TK.EZ : faast (LCMSMS)
|
-
|
|
|
1,4_Diaminobutan(**)
|
|
-
|
|
|
2_ Phenylethylamine(**)
|
|
|
|
|
Agramatine(**)
|
|
|
|
|
Cadaverine(**)
|
|
|
|
|
Histamine(**)
|
|
|
|
|
Tyramine(**)
|
|
|
|
|
Seprmine(**)
|
|
|
|
|
Serotonine(**)
|
|
|
|
|
Spermidine(**)
|
|
|
|
18.
|
Ester (Ethyl acetate) (**)
|
TK. AOAC 972.10 (GC/FID)
|
1.0mg/l
|
|
19.
|
Rượu bậc cao (Isobutanol, Isoamyl alcohol) (**)
|
TK. AOAC 972.10 (GC/FID)
|
1.0mg/l
|
|
20.
|
Aldehyd (Acetadehyd)(**)
|
TK. AOAC 972.10 (GC/FID)
|
2.0mg/l
|
|
21.
|
Furfural (**)
|
TK. AOAC 972.10 (GC/FID)
|
1.0mg/l
|
|
22.
|
Diacetyl(**)
|
TK. EPA 5021A (GCMS – HS)
|
0.2mg/l
|
|
23.
|
Các loại độc chất khác(**)
|
(GCMS)
|
-
|
|
24.
|
Các loại độc chất khác(**)
|
LCMSMS
|
-
|
|
25.
|
Hàm lượng các chất dễ bay hơi
có chứa nitơ, tính theo mg nitơ /l cồn 100o(**)
|
TK.TCVN 3706:1990
|
1 mg/L
|
|
IV. NITRIT AND NITRAT RESIDUES
|
|
26.
|
Nitrit (NO2-)(**)
|
TK.TCVN 7806:2007
|
1 mg/L
|
|
27.
|
Nitrat (NO3-)(**)
|
TK.TCVN 7806:2007
|
1 mg/L
|
|
V. METAL AND MICROELEMENTS
|
|
28.
|
Arsen (As)
|
AOAC 986.15 (2011)
|
0.01 mg/L
|
|
29.
|
Thủy ngân (Hg)(**)
|
AOAC 974.14 (2011)
|
0.01 mg/L
|
|
30.
|
Cadimi (Cd)
|
AOAC 999.11 (2011)
|
0.005 mg/L
|
|
31.
|
Chì (Pb)
|
AOAC 999.11 (2011)
|
0.01 mg/L
|
|
32.
|
Đồng (Cu)
|
AOAC 999.11 (2011)
|
0.2 mg/L
|
|
33.
|
Canxi (Ca)
|
AOAC 968.08 (2011)
|
0.5 mg/L
|
|
34.
|
Selen (Se)
|
AOAC 986.15 (2011)
|
0.01 mg/L
|
|
35.
|
Kali (K)
|
AOAC 969.23 (2011)
|
0.5 mg/L
|
|
36.
|
Magie (Mg)
|
AOAC 968.08 (2011)
|
0.5 mg/L
|
|
37.
|
Mangan (Mn)
|
AOAC 999.11 (2011)
|
0.5 mg/L
|
|
38.
|
Sắt (Fe)
|
AOAC 999.11 (2011)
|
0.5 mg/L
|
|
39.
|
Natri (Na)
|
AOAC 969.23 (2011)
|
0.5 mg/L
|
|
40.
|
Antimo (Sb)
|
TK.AOAC 986.15 (2011)
|
0.01 mg/L
|
|
41.
|
Kẽm (Zn)
|
AOAC 999.11 (2011)
|
0.5 mg/L
|
|
VI. VITAMIN
|
|
42.
|
Vitamin C
|
TK.AOAC 985.33:2011 (HPLC-UV)
|
0.1mg/l
|
|
43.
|
Vitamin B1
|
TK.AOAC 985.33:2011 (HPLC-UV)
|
0.1mg/l
|
|
44.
|
Vitamin B2
|
TK.AOAC 985.33:2011 (HPLC-UV)
|
0.1mg/l
|
|
45.
|
Vitamin B3 (Nicotinamide)
|
TK.AOAC 985.33:2011 (HPLC-UV)
|
0.1mg/l
|
|
46.
|
Vitamin B5 (Acid pantothenic)
|
TK.AOAC 985.33:2011 (HPLC-UV)
|
0.1mg/l
|
|
47.
|
Vitamin B6
|
TK.AOAC 985.33:2011 (HPLC-UV)
|
0.1mg/l
|
|
48.
|
Vitamin B9 (Folic acid)
|
TK.AOAC 985.33:2011 (HPLC-UV)
|
0.1mg/l
|
|
49.
|
Vitamin B12
|
TK.AOAC 985.33:2011 (HPLC-UV)
|
0.1mg/l
|
|
50.
|
Biotin(**)
|
TK.AOAC 985.33:2011 (HPLC-UV)
|
0.1mg/l
|
|
VII. PLANT PROTECTION DRUG RESIDUES
|
|
51.
|
Carbamate plant protection drug residues
|
TK.AOAC 2007.01 (LCMSMS)
|
ppb
|
|
|
Isoprocarb
|
ppb
|
|
|
Aldicarb sulfone
|
ppb
|
|
|
Aldicarb
|
ppb
|
|
|
Aldicarb sulfoxide
|
ppb
|
|
|
Propoxur
|
ppb
|
|
|
Carbofuran
|
ppb
|
|
|
Carbaryl
|
ppb
|
|
|
Methomyl
|
ppb
|
|
|
Oxamyl
|
ppb
|
|
|
Thiodicarb
|
ppb
|
|
|
Methiocarb
|
ppb
|
|
|
Fenobucarb
|
ppb
|
|
|
Propoxur
|
ppb
|
|
|
Carbofuran-3-Hydroxy
|
ppb
|
|
52.
|
Clo plant protection drug residues
|
ppb
|
|
|
4,4'-DDD
|
ppb
|
|
|
2,4'-DDD
|
ppb
|
|
|
4,4'-DDE
|
ppb
|
|
|
2,4'-DDE
|
ppb
|
|
|
4,4'-DDT
|
ppb
|
|
|
2,4'-DDT
|
ppb
|
|
|
Dieldrin
|
ppb
|
|
|
Aldrin
|
ppb
|
|
|
Alpha-Endosulfan
|
ppb
|
|
|
Beta-Endosulfan
|
ppb
|
|
|
Endrin
|
ppb
|
|
|
Alpha-HCH
|
ppb
|
|
|
Beta-HCH
|
ppb
|
|
|
Gamma-HCH
|
ppb
|
|
|
Isodrin
|
ppb
|
|
|
Heptachlor
|
ppb
|
|
|
Heptachlor epoxide
|
ppb
|
|
|
Hexachloro -Benzen
|
ppb
|
|
53.
|
Phosphor plant protection drug residues
|
ppb
|
|
|
Diazinon
|
ppb
|
|
|
Parathion Methyl
|
ppb
|
|
|
Malathion
|
ppb
|
|
|
Chlorpyrifos
|
ppb
|
|
|
Parathion ethyl
|
ppb
|
|
|
Bromophos methyl
|
ppb
|
|
|
Bromophos ethyl
|
ppb
|
|
|
Ethion
|
ppb
|
|
54.
|
Chrysanthemum plant protection drug residues
|
ppb
|
|
|
Cypermethrin
|
ppb
|
|
|
Deltamethrin
|
ppb
|
|
|
Permethrin
|
ppb
|
|
|
Fenvalerate
|
ppb
|
|
|
Resmethrine
|
ppb
|
|
|
Fenthropathrine
|
ppb
|
|
55.
|
Propargite(**)
|
TK.AOAC 970.52 (GCMS)
|
10.0mg/l
|
|
56.
|
Diphenylamine(**)
|
TK.AOAC 2007.01 (GCMS
|
50.0mg/l
|
|
VIII. FOOD ADDITIVES
|
|
57.
|
Phẩm màu(**)
|
TCVN 5517.1991
|
-
|
|
58.
|
Beta-caroten(**)
|
TK : AOAC 992.06 (HPLC/UV)
|
0.1mg/l
|
|
59.
|
Lycopen(**)
|
TK.AOAC 992.06:2011 (HPLC.UV)
|
0.1mg/l
|
|
60.
|
Orange II(**)
|
TK : LGC/GC/2007/005 Analysis of illegal
Dyes in chilli Powder by LC-UV (HPLC/UV
|
0.1mg/l
|
|
61.
|
Ponceau 4R(**)
|
TK : LGC/GC/2007/005 Analysis of illegal
Dyes in chilli Powder by LC-UV (HPLC/UV
|
10.0mg/l
|
|
62.
|
Sunset yellow(**)
|
TK : JFDA Vol 14, No3,
2006, P284 – 291 (HPLC/UV)
|
10.0mg/l
|
|
63.
|
Tartazine(**)
|
TK : JFDA Vol 14, No3, 2006,
P284 – 291 (HPLC/UV)
|
10.0mg/l
|
|
64.
|
Acid citric (E330)
|
Ref Megazyme International Ireland 2012
UHPLC-DAD
|
mg/L
|
|
65.
|
Acid Tartaric (E334)(**)
|
TK. US EPA method 300.00(IC)
|
20.0mg/L
|
|
66.
|
Acid malic (E296)(**)
|
TK. US EPA method 300.00(IC)
|
20.0mg/L
|
|
67.
|
Acid fumaric (E297)(**)
|
TK. US EPA method 300.00(IC)
|
20.0mg/L
|
|
68.
|
Acid lactic (E270)(**)
|
TK. US EPA method 300.00(IC)
|
20.0mg/L
|
|
69.
|
Acid ascorbic / Natri ascorbate
|
Ref Journal of Chromatography A
UHPLC-DAD
|
mg/L
|
|
70.
|
Acid acetic / Natri acetate(**)
|
TK. US EPA method 300.00(IC)
|
20.0mg/l
|
|
71.
|
BHA (Butylated hydroxyanisol)(**)
|
TK : AOAC 983.15 (HPLC/UV)
|
5.0mg/l
|
|
72.
|
BHT (Butylated hydroxytoluene)(**)
|
TK : AOAC 983.15 (HPLC/UV)
|
5.0mg/l
|
|
73.
|
TBHQ (Tert-Butyl hydroquinone)(**)
|
TK : AOAC 983.15 (HPLC/UV)
|
5.0mg/l
|
|
74.
|
Natri benzoate / Acid benzoic
|
Ref Journal of chromatography A, 1073(2005) 393 – 397
UHPLC-DAD
|
ppb
|
|
75.
|
Kali sorabte/ Acid sorbic
|
Ref Journal of Chromatography A
UHPLC-DAD
|
ppb
|
|
76.
|
Aspartame (E951)(**)
|
TK. TCVN 8471 : 2010 (HPLC/UV)
|
10.0mg/l
|
|
77.
|
Acesulfam K (E950)(**)
|
TK. TCVN 8471 : 2010 (HPLC/UV)
|
10.0mg/l
|
|
78.
|
Saccharine (E954)(**)
|
TK. TCVN 8471 : 2010 (HPLC/UV)
|
0.5mg/l
|
|
79.
|
Cyclamate (E952)(**)
|
TK. US EPA method 300.00(IC)
|
20.0mg/l
|
|
80.
|
Maltitol(**)
|
TK. GC - Chrompack application note,
Varian application 708
|
0.50%
|
|
81.
|
Mannitol(**)
|
TK. GC - Chrompack application note,
Varian application 708
|
0.50%
|
|
82.
|
Sorbitol(**)
|
TK. GC - Chrompack application note,
Varian application 708
|
0.50%
|
|
83.
|
Glucose(**)
|
TK. GC - Chrompack application note,
Varian application 708
|
0.50%
|
|
84.
|
Fructose(**)
|
TK. GC - Chrompack application note,
Varian application 708
|
0.50%
|
|
IX. MYCOTOXIN
|
|
85.
|
Aflatoxin Tổng(**)
|
TK.AOAC 991.31 (LC/MS/MS)
|
1.0µg/l
|
|
86.
|
Aflatoxin/chất (B1, B2, G1, G2)(**)
|
TK.AOAC 991.31(LC/MS/MS)
|
1.0µg/l
|
|
87.
|
Ochratoxin A(**)
|
TK. AOAC 2000.03(LC/MS/MS)
|
1.0µg/l
|
|
88.
|
Aflatoxin M1(**)
|
TK. AOAC 986.16:2002 (HPLC-UV)
|
0.01µg/l
|
|
89.
|
Patulin(**)
|
TK. TCVN 8161 : 2009 (LCMSMS)
|
20.0µg/l
|
|
X. MICROBIOLOGY
|
|
90
|
TPC
|
ISO 4833-1:2013
|
CFU/G
|
|
91
|
Coliform
|
ISO 4832:2006
|
CFU/G
|
|
92
|
E. coli
|
ISO 16649-2:2001
|
CFU/G
|
|
93
|
E. coli
|
ISO 7251:2005
|
MPN/G; /G
|
|
94
|
Staphylococcus positive coagulase
|
ISO 6888-1:1999
|
CFU/G
|
|
95
|
Staphylococcus aureus
|
ISO 6888-1:1999
|
CFU/G
|
|
96
|
Salmonella
|
ISO 6579:2002
|
/25G
|
|
97
|
Vibrio parahaemolyticus
|
ISO 21872-1:2007
|
/25G
|
|
98
|
Vibrio cholerae
|
ISO 21872-1:2007
|
/25G
|
|
99
|
Listeria monocytogenes
|
ISO 11290-1:1996/ Amd.1:2004
|
/25G
|
|
100
|
Total yeast - mould
|
ISO 21527-1&2: 2008
|
CFU/G
|
|
101
|
Clostridium perfringens
|
ISO 7937:2004
|
CFU/G
|
|
102
|
Spores of sulfite-reducing anaerobes (Clostridia)
|
ISO 15213:2003
|
CFU/G
|